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Nyheder (76)- AN-V-098AN-V-098Molybdenum in sulfuric acid
Mo is determined by polarography at the SMDE in nitric acid solution.
- AN-V-099AN-V-099Cadmium, lead, and copper in triphosphate
Cadmium, lead, and copper are determined by anodic stripping voltammetry (ASV) at the HMDE using aqueous nitric acid as supporting electrolyte.
- AN-V-100AN-V-100Nickel and cobalt in triphosphate
Ni and Co are determined in triphosphate by adsorptive stripping voltammetry (AdSV) in ammonia buffer at pH 9.5 with addition of dimethylglyoxime (DMG).
- AN-V-102AN-V-102Manganese in triphosphate
Anodic stripping voltammetry (ASV) at the HMDE is used to determine manganese in triphosphate. The sample is first digested and then measured in an alkaline solution.
- AN-V-103AN-V-103Chromium in lime (CaCO3)
Cr(VI) is determined at the HMDE in an electrolyte containing ethylenediamine and acetate. Because Cr(III) is electrochemically inactive, all Cr has to be oxidised prior to analysis.
- AN-V-104AN-V-104Formaldehyde in metalworking lubricants
Formaldehyde is determined polarographically at the DME in alkaline solution.
- AN-V-105AN-V-105Thallium in the presence of an excess of cadmium in zinc plant electrolytes (concentrated ZnSO4 solutions)
Thallium and cadmium can be determined by anodic stripping voltammetry (ASV) at the HMDE (Tl) and polarography at the DME (Cd), respectively using aqueous hydrochloric acid as supporting electrolyte. Since Cd is present in high excess and would therefore interfere with the determination of thallium, a post electrolysis procedure is applied to remove the co-deposited metal from the mercury drop.
- AN-V-106AN-V-106Nickel and cobalt in wastewater after UV digestion
Determination of nickel and cobalt in wastewater samples through adsorptive Stripping Voltammetry (AdSV). The wastewater samples first undergo a UV digestion in accordance with DIN 38406 Part 16.
- AN-V-107AN-V-107Tin in wastewater after UV digestion
Tin can be determined in wastewater by anodic stripping voltammetry (ASV) in oxalate buffer after addition of methylene blue. Samples with organic substances have to undergo UV digestion before analysis. Samples with higher concentrations of metals can be diluted before digestion.
- AN-V-108AN-V-108Thallium in wastewater after UV digestion
Thallium in wastewater is determined in acetate buffer in presence of EDTA by anodic stripping voltammetry (ASV). Samples with organic substances have to undergo UV digestion before analysis.
- AN-V-109AN-V-109Selenium in wastewater after UV digestion
Selenium is determined by cathodic stripping voltammetry (CSV) at the hanging mercury drop electrode (HMDE). Se(IV) is deposited on the surface of the mercury drop in sulfuric acid electrolyte under addition of copper ions as Cu xSe y.Wastewater samples containing organic contaminants have to be digested by UV irradiation before analysis. In addition, the sample has to undergo a second irradiation step at pH 7−9 to reduce Se(VI) to Se(IV), since only Se(IV) is electrochemically active.
- AN-V-110AN-V-110Total chromium in wastewater after UV digestion (polarography method with ethylene diamine)
Cr(VI) is determined by polarography at the SMDE in acetate solution containing ethylene diamine to mask interfering copper ions.Only Cr(VI) is electrochemically active. It is for that reason that all chromium compounds must be present before the analysis as CR(VI), which is guaranteed by UV radiation with a pH > 4.
- AN-V-111AN-V-111Germanium in zinc plant electrolytes (concentrated ZnSO4 solutions)
Germanium is determined by adsorptive stripping voltammetry (AdSV) at the HMDE using aqueous sulfuric acid as supporting electrolyte and pyrocatechol violet as complexing agent. It is possible to determine 20 µg/L Ge in a sample containing 150 g/L Zn, 3 g/L Cd and 1 mg/L Pb.
- AN-V-112AN-V-112Thiourea in nickel plating baths
Thiourea is determined by cathodic stripping voltammetry (CSV) at the HMDE in ammonia buffer at pH 8.9. Chloride in the sample does not interfere with this determination.
- AN-V-113AN-V-113Titanium in polyethylene terephthalate (PET)
Ti is determined in polyethylene terephthalate (PET) after digestion in sulfuric acid and hydrogen peroxide. Adsorptive stripping voltammetry (AdSV) with mandelic acid as complexing agent is used for this application.
- AN-V-114AN-V-114Cobalt in polyethylene terephthalate (PET)
Co is determined in polyethylene terephthalate (PET) after digestion in sulfuric acid and hydrogen peroxide. The application is carried out with adsorptive stripping voltammetry (AdSV) in ammonia buffer with dimethylglyoxime (DMG) as complexing agent.
- AN-V-115AN-V-115Antimony in polyethylene terephthalate (PET)
Sb is determined in polyethylene terephthalate (PET) after digestion in sulfuric acid and hydrogen peroxide. The application is carried out with anodic stripping voltammetry (ASV) in hydrochloric acid.
- AN-V-116AN-V-116Zinc and lead in ethanol
Zn and Pb are determined by anodic stripping voltammetry (ASV) in acetate buffer at pH 4.6.
- AN-V-117AN-V-117Iron in ethanol
Iron can be determined in ethanol by adsorptive stripping voltammetry (AdSV) at the HMDE. PIPES buffer is used as supporting electrolyte and catechol as complexing agent at a pH value of 7.0.
- AN-V-118AN-V-118Gold in ammonium thiosulfate solution
Gold can be determined by anodic stripping voltammetry (ASV) in the µg/l range at the Ultra Trace Graphite electrode. The solution should not contain halide ions.
- AN-V-120AN-V-120Nickel in ethylene glycol after UV digestion
The concentration of nickel in ethylene glycol can be determined by adsorptive stripping voltammetry (AdSV) after the organic matrix is destroyed by UV digestion.
- AN-V-121AN-V-121Total iron in wastewater after UV digestion (Triethanolaminebromate method)
The concentration of Fe(total) is determined in wastewater after UV digestion. The method is suitable for iron concentrations down to the low μg/L range. Stripping voltammetry is not applicable for this method. Fe(II) and Fe(III) generate signals with identical sensitivity.
- AN-V-122AN-V-122Iron (total) in deionized water (triethanolamine-bromate-method)
The concentration of Fe(total) is determined in deionized water. The method is suitable for iron concentrations down to the mid µg/L range. Electrochemical deposition is not applicable for this method. A subtraction of the reagent blank is recommended. Fe(II) and Fe(III) give signals with the same sensitivity.
- AN-V-123AN-V-123Iron (total) in ethylene glycol with 2,3 dihydroxynaphthalene
The concentration of Fe(total) is determined in monoethylene glycol by adsorptive stripping voltammetry with 2,3-dihydroxy-naphthalene as complexing agent. The detection limit of the method is approx. 0.1 µg/L with respect to the content in the measuring vessel. If no bromate is added to the supporting electrolyte the sensitivity of the method is about 10 times lower. All reagents have to be added in the order as listed below. Fe(II) and Fe(III) give signals with the same sensitivity. All reagents typically contain iron impurities, especially the 2,3-dihydroxy-naphthalene. Therefore a subtraction of the reagent blank is recommended.
- AN-V-124AN-V-124Iron(III) traces in standard solution with solochrome violet RS
The concentration of Fe(III) is determined by adsorptive stripping voltammetry with solochrome violet RS as complexing agent. All reagents have to be added in the order as listed below. Fe(II) does not show any signal. All reagents typically contain iron impurities. Therefore a subtraction of the reagent blank is recommended.
- AN-V-125AN-V-125Iron traces with 1-nitroso-2-naphthol
The concentration of Fe is determined in water samples by adsorptive stripping voltammetry with 1-nitroso-2-naphthol as complexing agent. All reagents have to be added in the order as listed below. All reagents typically contain iron impurities. Therefore a subtraction of the reagent blank is recommended. Fe(II) and Fe(III) show different sensitivities. Therefore the sample should only contain one of the iron species. Ascorbic acid (Vitamin C) can be added to the measuring solution and to the Fe(III) standard solution if both Fe(II) and Fe(III) are present in the sample to determine the concentration of total iron. A final concentration of ascorbic acid of 0.002 mol/L is suitable.
- AN-V-127Fe(II) in iron sucrose injection (USP)
Iron sucrose injection is a dark brown liquid which contains sucrose and iron(III) hydroxide in an aqueous solution, commonly used for the treatment of iron deficiency anemia. As a medical product, iron sucrose is subject to strict controls. Among other tests, the U.S. Pharmacopeia (USP) requires to monitor the limit of Fe(II) in the iron sucrose injection solution by polarography. The benefit of polarography is that Fe(II) and Fe(III) show signals at different potentials, and therefore an easier determination of Fe(II) without a previous separation of the two oxidation states is possible. The 884 Professional VA together with the viva software allows a straightforward determination of the Fe(II) content of iron sucrose injection solution following the requirements of the USP. The Fe(II) content is automatically calculated and stored in a database together with all relevant determination and calculation parameters.
- AN-V-128AN-V-128Iron (total) in a chromium electroplating bath
The concentration of Fe(total) is determined polarographically in a chromium electroplating bath. The method is suitable for iron in concentrations in the ppm range. Fe(II) and Fe(III) show signals with the same sensitivity.
- AN-V-129AN-V-129Iron (total) in phosphoric acid
The concentration of Fe is determined polarographically in phosphoric acid. The method is suitable for iron in concentrations in the ppm range. Fe(II) and Fe(III) show signals with the same sensitivity
- AN-V-130AN-V-130Aluminum in the ppb range in aqueous eluates of filter layers (Solochrome violet RS method)
The concentration of Al is determined by adsorptive stripping voltammetry at the HMDE. The method is suitable for Al in concentrations in the range of 0.1 ppb to approx. 40 ppb Al3+. Pb2+ ions do not interfere up to a concentration ratio Pb:Al = 10:1. Due to the slow complex formation of Al with solochrome violet RS the measuring solution was heated to 40 °C for 10 min prior to the determination. For standard addition a solution of Al with solochrome violet RS complex was used. All reagents have to be added in the order as listed below.
- AN-V-131AN-V-131Nickel and cobalt in sulfuric acid
The concentration of Ni and Co is determined by adsorptive stripping voltammetry at the HMDE with dimethylglyoxime (DMG) as complexing agent.
- AN-V-132AN-V-132Iron in sulfuric acid
The concentration of Fe is determined by adsorptive stripping voltammetry at the HMDE with 1-nitroso-2-naphthol (1N2N) as complexing agent.
- AN-V-133AN-V-133Suppressor «Copper Gleam 2001 Carrier» (Rohm and Haas) in acid copper bath
Determination of suppressor «Copper GleamTM 2001 Carrier» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-134AN-V-134Brightener «Copper Gleam 2001 Additive» (Rohm and Haas) in acid copper bath
Determination of brightener «Copper GleamTM 2001 Additive» in acid copper baths by modified linear approximation technique (MLAT) using cyclic voltammetric stripping (CVS).
- AN-V-135AN-V-135Suppressor «Cupracid BL-CT» (Atotech) in acid copper bath
Determination of suppressor «Cupracid BL-CT» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-136AN-V-136Brightener «Cupracid BL» (Atotech) in acid copper bath
Determination of brightener «Cupracid BL» in acid copper baths by linear approximation technique (LAT) using cyclicvoltammetric stripping (CVS).
- AN-V-137AN-V-137Suppressor «Cupraspeed» (Atotech) in acid copper bath
Determination of suppressor «Cupraspeed» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-138AN-V-138Brightener «Cupraspeed» (Atotech) in acid copper bath
Determination of brightener «Cupraspeed» in acid copper baths by modified linear approximation technique (MLAT)using cyclic voltammetric stripping (CVS).
- AN-V-140AN-V-140Antimony (total) in acid copper bath
The concentration of Sb(total) in an acid Cu bath is determined by anodic stripping voltammetry using hydrochloric acid as electrolyte. Due to the excess of Cu the deposition potential has to be chosen only 50 mV more negative than the Sb signal
- AN-V-141AN-V-141Suppressor «MACuSpec PPR 100 Wetter» Wetter (MacDermid) in acid copper bath
Determination of suppressor «MACuSpecTM PPR 100 Wetter» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-142AN-V-142Brightener «MACuSpec PPR 100» (MacDermid) in acid copper bath
Determination of brightener «MACuSpecTM PPR 100 Brightener» in acid copper baths by modified linear approximation technique (MLAT) using cyclic voltammetric stripping (CVS).
- AN-V-143AN-V-143Suppressor «Multibond 100 Part A20» (MacDermid) in acid copper bath
Determination of suppressor «MultiBondTM 100 Part A20» in an acid copper bath by dilution titration (DT) using cyclicvoltammetric stripping (CVS).
- AN-V-144AN-V-144Suppressor «Ronastan TP» (Rohm and Haas) in tin/lead bath
Determination of suppressor «Ronastan TP Additive» in a tin/lead bath by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-145AN-V-145Suppressor «Solderon ST-200 Primary» (Rohm and Haas) in a tin bath
Determination of suppressor «Solderon ST-200 Primary» in a tin bath by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-146AN-V-146Suppressor «InPulse H6» (Atotech) in acid copper bath
Determination of suppressor «InPulse H6» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-147AN-V-147Brightener «InPulse H6» (Atotech) in acid copper bath
Determination of brightener «InPulse H6» in acid copper baths by modified linear approximation technique (MLAT) using cyclic pulse voltammetric stripping (CPVS).
- AN-V-148AN-V-148Nickel in sulfamate-nickel plating bath
The concentration of Ni in a Ni plating bath is determined by polarography in ammonia buffer pH 9.6.
- AN-V-149AN-V-149Cobalt in sulfamate-nickel plating bath
The concentration of Co in a sulfamate Ni plating bath is determined by adsorptive stripping voltammetry (AdSV) inammonia buffer pH 9.6 with dimethylglyoxime (DMG) as complexing agent. All reagents have to be added in the order listed below. Special care has to be taken that the measuring solution is mixed well before the complexing agent is added. In case of precipitations of Ni-DMG further dilution of the sample is necessary.
- AN-V-150AN-V-150Copper in nickel plating bath
The concentration of Cu in a Ni plating bath is determined by polarography in chloride-containing acetate buffer at pH 4.7.
- AN-V-151AN-V-151Antimony(III) and antimony(total) in electroless nickel bath
The concentration of Sb(III) and Sb(total) in an electroless nickel bath is determined by anodic stripping voltammetry (ASV). In c(HCl) = 0.6 mol/L only Sb(III) shows a signal. In w(HCl) = 10% the Sb(total) content is determined.
- AN-V-152AN-V-152Thallium in cyanidic gold bath
The concentration of Tl in a cyanidic Au bath is determined by anodic stripping voltammety (ASV) without further addition of electrolyte.
- AN-V-154AN-V-154NTA in cyanidic gold bath
NTA in a cyanidic gold bath is determined as Bi-NTA complex by polarography. For standard addition a Bi-NTA standard solution is used.
- AN-V-155AN-V-155Suppressor «Thrucup EVF-B» (Uyemura) in acid copper bath
Determination of suppressor «Thru-Cup EVF-B» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-156AN-V-156Brightener «Thrucup EVF-1A» (Uyemura) in acid copper bath
Determination of brightener «Thru-Cup EVF-1A» in acid copper baths by modified linear approximation technique (MLAT) using cyclic voltammetric stripping (CVS).
- AN-V-157AN-V-157Leveler «Thru-Cup EVF-R» (Uyemura) in acid copper bath
Determination of leveler «Thru-Cup EVF-R» in acid copper baths by response curve technique (RC) using cyclic voltammetric stripping (CVS).
- AN-V-158AN-V-158Indium in a tin bath
The concentration of In in a Sn bath is determined in a HCl / Urotropin® containing electrolyte by anodic stripping voltammetry (ASV). The determination is linear up to approx. 0.5 mg/L with respect to the concentration of In in the measuring vessel. The standard addition solution is also prepared with HCl and Urotropin®.
- AN-V-159AN-V-159Bismuth in a tin bath
The concentration of Bi in a Sn bath is determined in a HCl / Urotropin® containing electrolyte by anodic stripping voltammetry (ASV). A reaction time of at least 25 min is required before the determination is started. The standard addition solution is also prepared with HCl and Urotropin®.
- AN-V-160AN-V-160Palladium in an activator
The concentration of Pd in an activator bath is determined by polarography in ammonium chloride electrolyte.
- AN-V-161AN-V-161Copper in a cyanidic copper bath
The concentration of Cu in a cyanidic Cu bath is determined by polarography.
- AN-V-162AN-V-162Iron in deoxidation solution (oxalate method)
The concentration of Fe(total) is determined by polarography in oxalate buffer pH 2. This method is suitable for iron concentrations in the mg/L range.
- AN-V-163AN-V-163Iron in degreasing bath
The concentration of Fe(total) is determined by polarography in an alkaline electrolyte containing triethanolamine (TEA) and KBrO3. All reagents typically contain iron impurities. Therefore a subtraction of the reagent blank is recommended.
- AN-V-164AN-V-164Titan in a titan pickle bath
The concentration of Ti in a Ti pickle bath is determined by polarography in an oxalic acid electrolyte.
- AN-V-165AN-V-165Zinc in phosphatation bath
The concentration of Zn in a zinc phosphatation bath is determined by polarography in ammonia buffer pH 9.3.
- AN-V-166AN-V-166Nickel in phosphatation bath
The concentration of Ni in a Zn phosphatation bath is determined by polarography in ammonia buffer pH 9.3.
- AN-V-167AN-V-167Cadmium in phosphatation bath
The concentration of Cd in a Zn phosphatation bath is determined by polarography in HCl electrolyte.
- AN-V-168AN-V-168Lead in phosphatation bath
The concentration of Pb in a Zn phosphatation bath is determined by anodic stripping voltammetry (ASV) in HCl electrolyte.
- AN-V-169AN-V-169Lead in tin soldering contacts
The concentration of Pb in Sn soldering contacts is determined by anodic stripping voltammetry (ASV) in an electrolyte containing citrate, oxalic acid, HCl, and cetyl trimethyl ammonium bromide.
- AN-V-170AN-V-170Selenium in zinc plant electrolyte
The concentration of Se(IV) in zinc plant electrolyte is determined by cathodic stripping voltammetry (CSV) in ammonium sulfate electrolyte containing EDTA and Cu. The Cu concentration has to be adapted to the sample and the deposition time. With voltammetry only free selenium is determined, therefore it has to be taken into consideration that selenium forms sparingly soluble compounds with numerous cations (e.g. Fe2(SeO3 )3 with Ks = 2·10-31).
- AN-V-171AN-V-171Tellurium in zinc plant electrolyte
The concentration of Te(IV) in Zn plant electrolyte is determined by cathodic stripping voltammetry (CSV) in ammonium sulfate electrolyte containing EDTA and Cu. To get a proper complexation of the interfering Zn a high amount of EDTA is necessary at pH 3.4.
- AN-V-172AN-V-172Cobalt in zinc plant electrolyte with a furildioxime as complexing agent
The concentration of Co in zinc plant electrolyte (neutral zinc sulfate solution) is determined by adsorptive stripping voltammetry (AdSV) in ammonia buffer with α-furildioxime as complexing agent.
- AN-V-173AN-V-173Lead in zinc sulfate solution
The concentration of Pb in zinc sulfate solution is determined by anodic stripping voltammetry (ASV) in hydrochloric acid electrolyte.
- AN-V-174AN-V-174Arsenic in zinc plant electrolyte
The concentration of As(total) in zinc plant electrolyte is determined by anodic stripping voltammetry (ASV) on a lateral gold electrode in HCl electrolyte. Due to the high excess of zinc in the sample the deposition potential has to be adapted. A second potential approx. 100 mV more negative than the arsenic signal has to be applied to selectively oxidize interfering antimony. For sample preparation the sample was passed through a cation exchange column to reduce the concentration of zinc in the measuring solution.
- AN-V-175AN-V-175Antimony(III) in zinc plant electrolyte with chloranilic acid as complexing agent
The concentration of of Sb(III) in zinc plant electrolyte is determined by adsorptive stripping voltammetry (AdSV) with chloranilic acid as complexing agent. In this method high copper concentrations do not interfere. An approx. 10-fold excess of lead interferes, since it shows a signal close to the antimony. With the parameters given below the working range of this method is 1 - 30 µg/L antimony(III) with respect to the concentration in the measuring vessel.
- AN-V-176AN-V-176Total selenium in drinking water after reduction of Se(VI) to Se(IV) with the 909 UV Digester
The Se(IV) concentration can be determined by cathodic Stripping Voltammetry (CSV) in an ammonium sulfate electrolyte. The analysis also functions in the presence of Cu. Se(IV) is determined in the first step. In order to register the entire content of Se, Se(VI) species are first reduced to Se(IV). This is handled by the 909 UV Digester at a pH value of between 7 and 9. The method requires practically no reagents and permits selenium speciation.
- AN-V-177AN-V-177Iron in a chromium bath (triethanolamine-bromate-method)
The concentration of Fe(total) is determined by polarography in alkaline electrolyte containing triethanolamine (TEA) and KBrO3. All reagents typically contain Fe impurities. Therefore a subtraction of the reagent blank is recommended.
- AN-V-178AN-V-178Copper in seawater with the Mercury Film Electrode (MFE)
The concentration of Cu in seawater is determined by anodic stripping voltammetry (ASV) in acetate buffer on a mercury film electrode (MFE). Gallium is added to overcome zinc interferences.
- AN-V-179Iron in boiler feed water
The iron concentration in boiler feed water has to be monitored to ensure reliable and safe operation of the water-steam circuit. Various guidelines set limits for the maximum iron content.The concentration of total iron in boiler feed water can be determined with high sensitivity using adsorptive stripping voltammetry (AdSV) using 2,3- dihydroxynaphthalene (DHN) as complexing agent. Voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) or inductive couple plasma (ICP) for the determination of iron with only a moderate investment in hardware required and low running costs.
- AN-V-180AN-V-180Nitrobenzene in aniline
The concentration of nitrobenzene in aniline is determined by polarography in an ethanol / acetic acid electrolyte.
- AN-V-181AN-V-181Chromium(VI) in cement
The concentration of Cr(VI) in cement is determined in tartrate electrolyte after acid extraction of the sample.
- AN-V-182AN-V-182Suppressor «Top Lucina a-M» (Okuno Chemical Industries) in acid copper bath
Determination of suppressor «Top Lucina α-M» in acid copper baths by dilution titration (DT) using cyclic voltammetric stripping (CVS).
- AN-V-183AN-V-183Brightener «Top Lucina a-2» (Okuno Chemical Industries) in acid Cu bath
Determination of brightener «Top Lucina α-2» in acid copper baths by modified linear approximation technique (MLAT) using cyclic voltammetric stripping (CVS).
- AN-V-184AN-V-184Leveler «Top Lucina a-3» (Okuno Chemical Industries) in acid Cu bath
Determination of leveler «Top Lucina α-3» in acid copper baths by response curve technique (RC) using cyclic voltammetric stripping (CVS).
- AN-V-185AN-V-185Cadmium and lead in electronic components as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of lead and cadmium in electronic components can be carried out by anodic stripping voltammetry (ASV) using ammonium oxalate buffer pH 2.
- AN-V-186AN-V-186Chromium(VI) in electronic components as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of chromium(VI) in electronic components can be carried out by polarography in ammonia buffer pH 9.6.
- AN-V-187AN-V-187Mercury in electronic components as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of mercury in electronic components can be carried out by anodic stripping voltammetry (ASV) at a gold rotating disk electrode (Au-RDE).
- AN-V-188AN-V-188Cadmium and lead in polymer materials as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of lead and cadmium in polymer materials can be carried out by anodic stripping voltammetry (ASV) using ammonium oxalate buffer pH 2.
- AN-V-189AN-V-189Chromium(VI) in polymer materials as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of chromium(VI) in polymer materials can be carried out by polarography in ammonia buffer pH 9.6.
- AN-V-190AN-V-190Mercury in polymer materials as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulatedheavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC62321 the determination of mercury in polymer materials can be carried out by anodic stripping voltammetry (ASV)at a gold rotating disk electrode (Au-RDE).
- AN-V-191AN-V-191Cadmium and lead in metallic materials as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of lead and cadmium in metallic materials can be carried out by anodic stripping voltammetry (ASV) using ammonium oxalate buffer pH 2.
- AN-V-192AN-V-192Chromium(VI) in chromate coating on metallic materials as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of chromium(VI) in chromate coating on metallic materials can be carried out by adsorptive stripping voltammetry (AdSV) using DTPA (diethylenetriamine pentaacetic acid) as complexing agent.
- AN-V-193AN-V-193Mercury in metallic materials as part of electrotechnical products
The EU directive on «Restriction of Hazardous Substances» (RoHS) requires the testing of four regulated heavy metals (Pb, Hg, Cd, Cr(VI)) in electrotechnical products. After sample preparation according to IEC 62321 the determination of mercury in metallic materials can be carried out by anodic stripping voltammetry (ASV) at a gold rotating disk electrode (Au-RDE).
- AN-V-194AN-V-194Copper in ethanol and fuel ethanol (E85) for car engines
The presence of copper in fuel ethanol blends has gained considerable attention since Cu2+ catalyzes oxidative reactions in gasoline leading to olefin decomposition and gum formation. Cu2+ in ethanol can easily be determined using anodic stripping voltammetry (ASV) in ethanol/gasoline blends without any sample pretreatment.
- AN-V-195Iodate in electroless nickel baths
Electroless nickel plating is an important and well established process in the surface finishing industry. In the past, the addition of small amounts of lead has widely been used to stabilize the plating bath. With the increasing number of restrictions in recent years on the use of lead in consumber products, particularly electronics, alternative stabilizers were developed and introduced. One of the stabilizers used as lead replacement is iodate. It can be used as a single additive or in combination with bismuth or antimony. This method allows the determination of iodate directly in the plating bath sample by polarography. The method is simple and fast, however, sensitive and robust.
- AN-V-196Antimony and bismuth in electroless nickel baths
Electroless nickel plating is an important and well established process in the surface finishing industry. In the past the addition of small amounts of lead has widely been used to stabilize the plating bath. With the increasing number of restrictions in recent years on the use of lead in consumber products, particularly electronics, alternative stabilizers were developed and introduced. Two of the stabilizers used as lead replacement are antimony and bismuth. They can be used as a single additive or in combination with each other or iodate. This method allows the determination of antimony and bismuth directly in the plating bath sample by anodic stripping voltammetry (ASV). The method is simple and fast, however sensitive and robust
- AN-V-197Indirect determination of iodide in brine with stripping voltammetry
It is crucial to monitor iodide in NaCl brine to prevent membrane fouling during chlor-alkali electrolysis. Stripping voltammetry offers precise iodide analysis.
- AN-V-198AN-V-198Aluminum in drinking water by adsorptive stripping voltammetry using alizarin red S (DASA) as complexing agent
Aluminum can be determined in drinking water by adsorptive stripping voltammetry at the HMDE using alizarin red S (DASA) as complexing agent. The method is linear up to 35 μg/L. The detection limit for this method is β(Al) = 1 μg/L, the limit of quantification is β(Al) = 3 μg/L. The sensitivity of the method cannot be increased by deposition.
- AN-V-199Voltammetric determination of gold(I) in gold plating baths
Controlling Au(I) levels in gold plating baths is required for high quality. Voltammetric analysis with the Multi-Mode Electrode Pro is an efficient solution.
- AN-V-200Determination of thiourea in copper electrorefining solutions
Thiourea measurement during copper electrorefining can be complicated by high chloride levels. Voltammetric analysis overcomes this issue, improving copper quality.
- AN-V-201AN-V-201Nickel and cobalt in red wine after UV digestion
The determination of nickel and cobalt in red wine using adsorptive stripping voltammetry can be carried out after UV digestion of the sample.
- AN-V-202AN-V-202Determination of suppressor in acid copper baths by smartDT
The determination of suppressor with dilution titration (DT) involves numerous additions with standard solution or sample to reach the evaluation ratio. Usually fixed, equidistant addition volumes are used. With smartDT, variable addition volumes are used that are automatically calculated by the software. At the beginning, the volumes are bigger. Towards the evaluation ratio, the addition volume becomes smaller to guarantee a good accuracy of the result. The operator defines the first and the smallest addition volume to be used. All volumes in between are calculated by the software considering the progress of the determination. Using smartDT with intelligent addition volumes, the determination of suppressor can be significantly accelerated with the same or even better accuracy than with the classic DT. The time saving per determination is between 20 and 40%.
- AN-V-203AN-V-203Determination of copper in electrolyte solutions for production of CIGS solar cells
This Application Note describes the polarograhic determination of copper in electroplating baths used in the production of thin-film copper indium gallium diselenide solar cells (CIGS cells). The CIGS absorber layer is electrodeposited on a molybdenum-coated substrate.Copper analysis is carried out after dilution of the sample with sulfuric acid as supporting electrolyte.
- AN-V-204AN-V-204Determination of indium in electrolyte solutions for production of CIGS solar cells
This Application Note describes the polarographic determination of indium in electroplating baths used in the production of copper indium gallium diselenide thin-film solar cells (CIGS cells). The CIGS absorber layer is electrodeposited on the molybdenum-coated substrate. Indium analysis is carried out after dilution of the bath sample with sulfuric acid as supporting electrolyte.
- AN-V-205AN-V-205Determination of gallium in electrolyte solutions for production of CIGS solar cells
This Application Note describes the determination of gallium in electroplating baths used in the production of copper indium gallium diselenide thin-film solar cells (CIGS cells). The CIGS absorber layer is electrodeposited on a molybdenum-coated substrate. Gallium analysis using anodic stripping voltammetry (ASV) is carried out after dilution of the sample with sulfuric acid as supporting electrolyte.
- AN-V-206AN-V-206Determination of selenite in electrolyte solutions for production of CIGS solar cells
This Application Note describes the polarographic determination of selenite in electroplating baths used in the production of copper indium gallium diselenide thin-film solar cells (CIGS cells). The CIGS absorber layer is electrodeposited on a molybdenum-coated substrate. Selenite analysis is carried out after dilution of the sample with sulfuric acid as supporting electrolyte.
- AN-V-207AN-V-207Determination of cadmium in electrolyte solutions for production of CIS and CIGS solar cells
This Application Note describes the polarographic determination of cadmium in electroplating baths used in the production of copper indium gallium diselenide (CIGS) or copper indium diselenide thin-film solar cells (CIS). Cadmium sulfide (CdS) from the electrolyte solution is deposited as a thin film on the CIS or CIGS absorber layer via chemical bath deposition (CBD).
- AN-V-208AN-V-208Determination of thiourea in electrolytes for production of CIS and CIGS solar cells
This Application Note describes the polarographic determination of thiourea in electroplating baths used in the production of copper indium gallium diselenide (CIGS) or copper indium diselenide thin-film solar cells (CIS). Cadmium sulfide (CdS) from the electrolyte solution is deposited as a thin film on the CIS or CIGS absorber layer via chemical bath deposition (CBD).
- AN-V-209Carbonyl test methods for alcohols
This polarographic method uses the Multi-Mode Electrode Pro for simultaneous detection of carbonyl impurities in alcohols, ensuring high product quality and stability.
- AN-V-210Total arsenic in mineral water
Arsenic is ubiquitous in the earth’s crust in low concentrations. Elevated levels can be found in mineral deposits and ores. Arsenic from such deposits leaches into the groundwater in the form of arsenite (AsO33–) and arsenate (AsO43–), causing its contamination. In addition to the arsenic originating from natural sources, industry and agriculture contribute to the contamination to a lower extent. The guideline value for inorganic total arsenic in the World Health Organization’s «Guidelines for Drinking-water Quality» is set to 10 μg/L. With a limit of detection (LOD) of 0.9 μg/L, anodic stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) for the determination of arsenic. While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetry can be used conventionally in the laboratory or alternatively in the field using the 946 Portable VA Analyzer. The determination is carried out on the scTRACE Gold electrode.
- AN-V-211Arsenic(III) in mineral water
Arsenic is ubiquitous in the earth’s crust in low concentrations. Elevated levels can be found in mineral deposits and ores. Arsenic from such deposits leaches into the groundwater in the form of arsenite (AsO33–) and arsenate (AsO43–), causing its contamination. As(III) is more toxic than As(V) and shows higher mobility in the environment. The selective determination of this species is possible using the method described in this document.With a limit of detection (LOD) of 0.3 μg/L, anodic stripping voltammetry allows speciation, i.e. the specific determination of As(III). While atomic absorption spectroscopy (AAS) (and competing methods) can only determine the total element concentration, anodic stripping voltammetry is selective to the As(III) oxidation state. The determination is carried out on the scTRACE Gold electrode.
- AN-V-212Mercury in mineral water
Mercury and its compounds are toxic. The highest risk is posed by chronic poisoning with mercury compounds ingested with food. A significant part of the mercury present in the environment is of anthropogenic origin. Considerable sources are coal-fired power plants, steel, and nonferrous metal production, waste incineration plants, the chemical industry, or artisanal gold mining where the use of elemental mercury for the extraction of gold from the ore is still common. The guideline value for inorganic mercury in the World Health Organization’s «Guidelines for Drinking-water Quality» is set to 6 μg/L.With a limit of detection (LOD) of 0.5 μg/L, anodic stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS).While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetry can be used conventionally in the laboratory or alternatively in the field with the 946 Portable VA Analyzer. The determination is carried out on the scTRACE Gold electrode.
- AN-V-213Copper in drinking water
Higher levels of copper in drinking water are usually caused by corrosive action of water leaching copper from copper pipes. While copper is an essential nutrient for the human organism, ingestion of higher concentrations have an adverse effect on human health. The current World Health Organization’s «Guidelines for Drinking-water Quality» recommend a maximum concentration of 2000 μg/L. With a limit of detection (LOD) of 0.5 μg/L, anodic stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) for the determination of copper in drinking water. While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetry can be used conventionally in the laboratory or alternatively in the field with the 946 Portable VA Analyzer. The determination is carried out on the scTRACE Gold electrode.
- AN-V-214Lead in drinking water
Lead is known to be highly toxic to humans as it interferes with enzyme reactions. Chronic lead poisoning can be caused by lead leaching into drinking water from piping systems. The current provisional guideline value in the World Health Organization’s «Guidelines for Drinking-water Quality» sets a maximum concentration of 10 μg/L. With a limit of detection (LOD) of 0.2 μg/L, anodic stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) to determine lead in drinking water. While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetry can be used conventionally in the laboratory or alternatively in the field with the 946 Portable VA Analyzer. The determination is carried out on a silver film applied to the scTRACE Gold electrode.
- AN-V-215Zinc in drinking water with the scTRACE Gold
Zinc is an essential trace element for humans. Excessive intake of zinc in higher concentrations can be harmful, however. There is no guideline value for zinc in the World Health Organization’s «Guidelines for Drinking-water Quality» because typical levels usually found in drinking water are of no concern. Anodic stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) for the determination of zinc in drinking water. While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetric determinations can be used conventionally in the laboratory or alternatively in the field using with 946 Portable VA Analyzer. The determination is carried out on the scTRACE Gold electrode.
- AN-V-216Iron in drinking water
Iron is an essential element in human nutrition. It can be present in drinking water as a result of water treatment or from corrosion in the water piping system. There is no guideline value for iron in the World Health Organization’s «Guidelines for Drinking-water Quality» because typical levels usually found in drinking water are of no concern. However, there are national limit values in various countries. The European Union has set a guideline indicator value for iron of 200 μg/L. Voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) for the determination of iron in drinking water. While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetric determinations can be done used conventionally in the laboratory or alternatively in the field using the with 946 Portable VA Analyzer. The determination is carried out with adsorptive stripping voltammetry (AdSV) using 2,3-dihydroxynaphthalene (DHN) on the scTRACE Gold electrode.
- AN-V-217Nickel, cobalt in drinking water
Nickel is widely used in stainless steel production. At high enough concentrations, it is known to cause allergic reactions when in contact with skin. Drinking water may be contaminated by taps which are made from metals containing nickel. The guideline value for nickel in the World Health Organization’s «Guidelines for Drinking-water Quality» is set to 70 μg/L. National limit values of typically lower at e. g. 20 μg/L. Cobalt usually occurs associated with nickel and can be found in smaller concentrations besides nickel. Adsorptive stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) for the determination of nickel and cobalt in drinking water. While AAS (and competing methods) can only be performed in a laboratory, adsorptive stripping voltammetric determinations can be used in the laboratory or alternatively in the field with the 946 Portable VA Analyzer. The determination is carried out on a bismuth film applied to the scTRACE Gold electrode.
- AN-V-218Bismuth in drinking water
Bismuth is considered as a metal with a very low toxicity. In high concentrations toxic effects have been described, however. There is no guideline value for bismuth in the World Health Organization’s «Guidelines for Drinking-water Quality» because typical levels usually found in drinking water are of no concern. Anodic stripping voltammetry is a viable, less sophisticated alternative to atomic absorption spectroscopy (AAS) for the determination of bismuth in drinking water. While AAS (and competing methods) can only be performed in a laboratory, anodic stripping voltammetry can be used in the laboratory or alternatively in the field with the 946 Portable VA Analyzer. The determination is carried out on the scTRACE Gold electrode.
- AN-V-219Sn(II) in radiopharmaceuticals
Sodium pertechnetate (99mTc) radiopharmaceuticals are widely used in medical imaging diagnostic procedures to help diagnose a large number of diseases affecting the bones and major organs. These radiopharmaceuticals are usually prepared from cold kits consisting of several ingredients, including a reducing agent. Sn(II) is a typical reducing agent which reduces the Tc(VII) that is added to the cold kit to a lower oxidation state which then forms the stable organic complex.For quality control, the tin content has to be determined in the kit vial. Sn(II) can be selectively determined using differential pulse polarography. Polarography is a straightforward, sensitive, selective, and interference-free method for the determination of mg/L levels of Sn(II) in radiopharmaceuticals.
- AN-V-220Remaining Useful Life of lubricants
Testing of in-service lubricating oils for their remaining antioxidant content is critical for capital equipment uptime as well as reducing running costs and repair expenses. Test methodologies such as RPVOT (rotating pressure vessel oxidation test) are time consuming and expensive to perform. Remaining Useful Life is a proven voltammetric method for testing the remaining active antioxidant content in minutes. Depending on the electrolyte, aromatic amine and phenolic antioxidants or hindered phenolic antioxidants can be determined.For the first time, a fully automated system is demonstrated, showing dramatically improved repeatability of data for confidence in reporting. Operator time is saved during sample preparation and irreproducible manual interpretation is eliminated via completely autonomous software processing. The user adds the sample into the vials, then the determination process of the sample series (including sample preparation and result calculations) is carried out automatically. The system is based on methods ASTM D6810, ASTM D6971, ASTM D7527, and ASTM D7590.
- AN-V-221Cadmium and lead in drinking water with a Bi drop electrode
To reduce the toxic effects of cadmium on the human body, as well as to limit the neurotoxic effects of lead, the provisional guideline values in the World Health Organization’s «Guidelines for Drinking-water Quality» are set to a maximum concentration of 3 µg/L for cadmium and 10 µg/L for lead. The completely mercury-free Bi drop electrode takes the next step towards converting voltammetric analysis into a non-toxic approach for heavy metal detection. Using this environmentally friendly sensor for anodic stripping voltammetry (ASV) allows the simultaneous determination of Cd and Pb in drinking water. The outstanding sensitivity is more than sufficient to monitor the provisional WHO guideline values.
- AN-V-222Iron determination in drinking water
The presence of iron in drinking water can lead to an unpleasant taste, stains, or even growth of «iron bacteria» that can clog plumbing and cause an offensive odor. Over a longer period, the formation of insoluble iron deposits is problematic in many industrial and agricultural applications. To avoid these problems, the U.S. Environmental Protection Agency (EPA) defines the Secondary Maximum Contaminant Level (SMCL) for water treatment and processing plants as 0.3 mg/L Fe in drinking water.The voltammetric determination of the iron triethanolamine complex on the non-toxic Bi drop electrode allows both the detection at very low levels (limit of detection of 0.005 mg/L) and measurements in a wide range of concentrations up to 0.5 mg/L.
- AN-V-223Nickel and cobalt in drinking water with a Bi drop electrode
The main sources of nickel pollution are electroplating, metallurgical operations, or leaching from pipes and fittings. Catalysts for the petroleum and chemical industries are major application fields for cobalt. In both cases, the metal is either released directly, or via the waste water-river pathway into the drinking water system. Therefore in the EU the legislation specifies 20 µg/L as the limit value for the Ni concentration in drinking water.The simultaneous and straightforward determination of nickel and cobalt is based on adsorptive stripping voltammetry (AdSV). The unique properties of the non-toxic Bi drop electrode combined with AdSV results in an excellent performance in terms of sensitivity.
- AN-V-224Nickel and cobalt in drinking water with a glassy carbon electrode
Due to the toxicity and the detrimental effects of nickel and cobalt on human health, their concentrations in drinking water must be controlled. Therefore, EU the legislation specifies 20 µg/L as the limit value for nickel in drinking water. The current provisional guideline value for Ni in the World Health Organization’s «Guidelines for Drinking-water Quality» is set to a maximum concentration of 70 µg/L. To monitor the concentrations of Ni and Co with the 884 Professional VA, a method for simultaneous determination on the glassy carbon electrode (GC-RDE) modified with a Bi film is used.
- AN-V-225Cadmium and lead in drinking water with a glassy carbon electrode
To reduce the toxic effects of cadmium on the kidneys, skeleton, and the respiratory system, as well as the neurotoxic effects of lead, the provisional guideline values in the World Health Organization’s (WHO) «Guidelines for Drinking-water Quality» are set to a maximum concentration of 3 µg/L for cadmium and 10 µg/L for lead.The powerful anodic stripping voltammetry (ASV) technique on the ex-situ mercury film modified glassy carbon electrode is more than sufficient to monitor the proposed WHO guidelines for Cd and Pb in drinking water.
- AN-V-226Zinc in drinking water with a glassy carbon electrode
No health-based guideline value exists for zinc. However, to maintain good quality municipal drinking water, the United States Environmental Protection Agency (US-EPA) set a maximum concentration of 5 mg/L as the limit value. Typical concentrations in surface and ground waters are between 10–40 μg/L Zn, with values up to 1 mg/L in tap water. Anodic stripping voltammetry (ASV) on the ex-situ mercury film modified glassy carbon electrode provides a less complex alternative to atomic absorption spectroscopy (AAS) for zinc determination in drinking water.
- AN-V-227Chromium(VI) in drinking water with a glassy carbon electrode
The guideline value for chromium in the World Health Organization’s (WHO) «Guidelines for Drinking-water Quality» is 50 µg/L. It should be noted here that chromium concentrations are often expressed as total chromium and not as chromium(III) or (VI). Chromium(VI) is responsible for changes in genetic material, and is found in significantly lower concentrations than Cr(III). Therefore an extremely sensitive method is required to monitor Cr(VI) in drinking water.The powerful adsorptive stripping voltammetry (AdSV) technique on the ex-situ mercury film modified glassy carbon electrode using DTPA as complexing agent can be used to determine such low concentrations.
- AN-V-228Thallium in drinking water
Presence of thallium in surface water is an indicator of industrial effluents and poses a serious health hazard if imbibed. Monitoring of thallium concentration can easily be done with anodic stripping voltammetry on the silver film modified scTRACE Gold. This non-toxic method allows the determination of thallium concentrations between 10–250 µg/L and can be carried out with the 946 Portable VA Analyzer.
- AN-V-229Antimony(III) in drinking water
The toxicity of antimony depends on its oxidation state: antimony(III) is more toxic than antimony(V). Due to its carcinogenicity, EU legislation specifies 5 µg/L and the World Health Organization (WHO) sets a maximum concentration of 20 µg/L as the Sb(III) limit value in drinking water.Straightforward determination using anodic stripping voltammetry provides a fast (analysis time under 10 minutes) and an ultra-sensitive tool for monitoring the antimony(III) concentration in drinking water. Measurements can be performed in the laboratory with the 884 Professional VA, or alternatively in the field with the 946 Portable VA Analyzer.
- AN-V-230Chromium(VI) in drinking water with the scTRACE Gold
The guideline value for total chromium in the World Health Organization’s (WHO) «Guidelines for Drinking-water Quality» is 50 µg/L. Chromium(VI) is more toxic than its trivalent form (Cr(III)) and is also less abundant. Therefore a robust and sensitive method is required to monitor its concentration in drinking water. The mercury film modified scTRACE Gold can be used to monitor chromium(VI), offering easy handling and a high grade of stability.
- AN-V-231Cadmium and lead in drinking water with screen-printed carbon electrodes
The provisional guideline values in the World Health Organization’s (WHO) «Guidelines for Drinking-water Quality» are set to 3 µg/L for cadmium and 10 µg/L for lead. The anodic stripping voltammetry (ASV) technique performed on the ex-situ mercury film modified Metrohm DropSens screen-printed electrode (SPE) can be used to simultaneously detect concentrations as low as 0.3 µg/L for both elements. This is suitable to monitor the WHO guideline values. The main advantage of this method lies in the innovative and cost-effective screen-printed electrode.
- AN-V-232Nickel and cobalt in drinking water with screen-printed carbon electrodes
EU legislation specifies 20 µg/L as the limit value for nickel in drinking water. The current provisional guideline value for Ni in the World Health Organization’s «Guidelines for Drinking-water Quality» is set to a maximum concentration of 70 µg/L. The adsorptive stripping voltammetry (AdSV) technique performed on the ex-situ bismuth film modified Metrohm DropSens 11L screen-printed electrode (SPE) can be used to simultaneously detect concentrations as low as 0.4 µg/L for nickel and 0.2 µg/L for cobalt with a 30 s deposition time.The disposable, maintenance-free sensor can be used conventionally in the laboratory with the 884 Professional VA, or alternatively in the field with the 946 Portable VA Analyzer. This method is best suited for manual systems.
- AN-V-233Selenium(IV) in drinking water
The difference between the toxic and essential levels of selenium to human health are very slight. Therefore, the current provisional guideline value for selenium(IV) in the World Health Organization’s «Guidelines for Drinking-water Quality» and in the European Drinking Water Directive is set to a maximum concentration of 10 µg/L.The anodic stripping voltammetric (ASV) technique performed on the unmodified scTRACE Gold can be used to determine concentrations as low as 0.5 µg/L selenium with a 30 s deposition time. These limits can be lowered even further by increasing the deposition time. The linear range at 30 s deposition time ends at approximately 100 μg/L. The scTRACE Gold electrode does not need extensive maintenance such as mechanical polishing. Measurements can be performed in the laboratory with the 884 Professional VA or alternatively in the field with the 946 Portable VA Analyzer. This method is suited for manual or automated systems.
- AN-V-234Tellurium(IV) in drinking water
Tellurium is one of the elements recently identified as technologically critical for photovoltaic conversion, quantum dots, as well as in thermoelectric technology, and has the potential to become a new emergent contaminant. Until now there is no guideline value in the World Health Organization’s «Guidelines for Drinking-water Quality» and in the European Drinking Water Directive for tellurium(IV) concentration in drinking water.To monitor the tellurium(IV) levels in drinking water, anodic stripping voltammetry (ASV) performed on the unmodified scTRACE Gold is recommended. This method allows determination of tellurium(IV) in the concentration range between 1 µg/L and 60 µg/L when using a 90 s deposition time. The scTRACE Gold electrode does not need extensive maintenance such as mechanical polishing. Measurements can be performed in the laboratory with the 884 Professional VA or alternatively in the field with the 946 Portable VA Analyzer.
- AN-V-235Cadmium in chocolate
The toxic element cadmium (Cd) can be found in elevated concentrations with high bioavailability in some soils. Under such conditions, cacao trees can accumulate cadmium in the beans, which are then processed into cocoa. Chocolate produced from the affected beans will contain elevated cadmium levels. Typical limit values in the European Union are between 100 µg/kg and 800 µg/kg (EU Commission Regulation 1881/2006) depending on the cocoa content of the chocolate.Anodic stripping voltammetry (ASV) can be used to accurately determine trace quantities of cadmium in chocolate down to approximately 10 µg/kg. The method is simple to perform, specific, and free of interferences. Prior to determination the samples are ashed in a furnace at 450 °C.
- AN-V-236Antimony stabilizer in an electroless Ni bath
Monitoring Sb(III) stabilizer levels during electroless Ni plating is critical for high-quality coatings. Anodic stripping voltammetry offers fast, reliable Sb(III) analysis.
- AN-V-237Lead stabilizer in an electroless Ni plating bath
Electroless nickel plating ensures low-cost wear and corrosion resistance. Monitoring lead stabilizer levels in Ni plating baths is possible with the Bi drop electrode.
- AN-V-238Bismuth stabilizer in an electroless Ni plating bath
Electroless Ni plating offers superior surface finish and corrosion resistance. Anodic stripping voltammetry allows Bi stabilizer to be monitored in Ni plating baths.
- AN-V-239Iron speciation in LiFePO4 batteries
Lithium iron phosphate batteries offer users safety and durability. Polarographic speciation evaluates Fe(II) and Fe(III) in cathode material, useful for several tests.
- AN-V-240Determination of total iodine in thyroid tablets with polarography
Accurate iodine determination in thyroid tablets, ensuring treatment efficacy, is achieved using the 884 Professional VA and Multi-Mode Electrode pro per USP guidelines.
- AN-V-241Fe(II)/Fe(III) speciation in iron citrate capsules by voltammetry
The total iron content as well as the distribution of Fe(II) and Fe(III) are critical quality attributes for iron citrate. Conventional techniques such as ICP and mass spectrometry do not directly distinguish iron species without additional sample preparation. This study shows how voltammetry enables direct, selective quantification of Fe(II) and Fe(III) in citrate matrices, while standard addition compensates for matrix effects to ensure reliable results.
- AN-V-242brightRC – Advanced brightener analysis with a response curve
brightRC enables reliable CVS (or CPVS) brightener quantification without repeated standard additions, especially for additive systems with nonlinear signal behavior. By using external response curve (RC) calibration and flexible regression, it avoids systematic errors inherent to linear standard addition methods and significantly reduces analysis time. This makes brightRC ideal for high throughput routine control in stable copper plating baths.
- BWT-4901BWT-4901Raman Spectroscopy for Quick Quality Analyis of Diamond Membranes
Portable Raman is used to characterize the quality of diamond foils made by CVD processes.
- BWT-4902BWT-4902Raman Analysis of Si Crytallinity
Raman spectroscopy at 532 nm excitation is used to study the crystalline and amorphous content of mixed phase silicon films.
- BWT-4903BWT-4903The NanoRam Hand-held Raman Spectrometer: Ideally-suited for the Inspection of Raw Materials and Chemicals Used in the Pharmaceutical industry
The NanoRam handheld Raman, with a TE-cooled spectrometer, and patented CleanLaze technology packaged in a small, touch-screen operating unit, delivers high quality raw material testing capabilities for pharmaceutical manufacturers.
- BWT-4904BWT-4904The Benefits of Raman Spectroscopy for the Identification and Characterization of Polymers
Raman spectroscopy is a quick nondestructive method for the direct identification of plastics. It can also be used for the analysis of flame retardants, lubricants and other additives. Coupled with chemometric software, quantitative and advanced qualitative analyses can be performed.
- BWT-4905BWT-4905The NanoRam Hand-held Raman Spectrometer Full Regulatory Compliance for the Inspection of Raw Materials and Chemicals Used in the Pharmaceutical Industry.
The NanoRam is a state-of-the-art, handheld Raman spectrometer for the rapid identification of chemicals used in the pharmaceutical manufacturing process. It has been specifically designed for these applications and is fully compliant with all the major global regulatory, safety, and commercial testing agencies applicable to the pharmaceutical industry.
- BWT-4906BWT-4906Rapid Raw Material Identification for Formulation Compounds Using Handheld Raman Technology
The raw materials whey, sorbitol, stearic acid, and calcium phosphate dihydrate dibasic all show very distinctive, unique Raman signatures, which indicates that Raman spectroscopy is the ideal technology for identification of these materials. The PCA model-based method provides reliable specificity to successfully identify these nondestructively in plastc samples bags using the NanoRam.
- BWT-4907BWT-4907Fundamentals of Raman Spectroscopy
The fundamentals of Raman instrumentation and spectroscopy are presented along with common applications of Raman.
- BWT-4908BWT-4908The Benefits of a High-Performance Handheld Raman Spectrometer for the Rapid Identification of Pharmaceutical Raw Materials
The principles and benefits of Raman are presented in terms of advances that make handheld Raman an integral tool for pharmaceutical manufacturers to comply with incoming material testing requirements. Examples of the NanoRam for positive identification of excipients including celluloses and sugars illustrate the selectivity of Raman.
- BWT-4909BWT-4909The Use of Raman Spectroscopy in the Field of Cancer Diagnostics
Raman spectroscopy and surface enhanced Raman spectroscopy (SERS) are proving to be invaluable tools in the field of biomedical research and clinical diagnostics. Raman systems are also being developed for molecular diagnostic testing to detect and measure human cancer biomarkers. This review highlights two applications realting to breast cancer and pancreatic cancer diagnosis together with examples of the use of Raman spectrometry in biomedical research areas such as the identification of bacterial infections, showing that Raman is an important part of the medical toolbox, as we continually strive to improve diagnostic techniques and bring a better health care system to patients.
- BWT-4910BWT-4910The Use of Portable and Handheld Raman for Forensic Investigations
Today's Raman instrumentation is faster, more rugged, and less expensive than in the past and the advances in component miniaturization have led to the design of portable devices with extremely high performance designed for field-based investigations. This study focuses on the use of handheld Raman spectroscopy for the characterization and identification of samples encountered in various application areas related to forensic science.
- BWT-4911BWT-4911Using Handheld Raman to Reduce Risks in Materials Used for Manufacturing
Raman spectroscopy is a valuable tool to provide rapid, specific analysis for identification of raw materials, thus reducing the risk of using substandard or incorrect materials in manufacturing. The utility of handheld Raman increases productivity, and the ability to do full testing without creating bottlenecks in the production process. The integration of the Raman data into a company’s data management system provides a secure means of handling data and results, with reduced risk of transcription errors, and data loss.
- BWT-4912BWT-4912Quantitative Analysis Using New Generation Raman Spectrometers and Chemometrics ─ Smaller and Faster
Small, fast high-performance Raman spectrometers are now readily available. Three real-life Raman quantitative and semi-quantitative analysis applications are discussed. These applications showcase the versatility of Raman spectroscopy and the potential impact that it can make in various industries such as security, pharmaceutical, and plastics and polymers.
- BWT-4913BWT-4913The Versatility of Portable Raman in Process Development
Raman spectroscopy is a well suited spectroscopic technique for process development and control within development laboratories in chemical, pharmaceutical, and other industries. This article demonstrates the utility of portable Raman spectroscopy as a simple and versatile tool for in situ monitoring of reactions using univariate analysis techniques such as peak trending, as well as multivariate analysis approaches to predict the end point of chemical reactions.
- BWT-4914BWT-4914Raman Spectroscopy Peers Through Packaging
Patented STRaman technology is a new Raman technique that can identify chemical species nondestructively beneath diffusely scattering packaging material such as plastics or tablet coatings.
- BWT-4915BWT-4915Portable, High-Efficiency Transmission Raman Spectroscopy for At-Line Content Uniformity Testing of Pharmaceutical Tablets
Content uniformity of solid dosage forms can be done nondestructively at the process line using the QTRam portable transmission Raman system.
- BWT-4916BWT-4916See-Through Science
Allowing non-destructive chemical identification through opaque materials, award-winning STRam represents an evolution in Raman technology.
- EB-001EB-001Near-infrared spectroscopy for the analysis of petrochemicals
Improve petrochemical quality control with NIRS. Fast, cost-effective, and no sample prep needed. Learn more in our eBook.
- EB-002EB-002NIR spectroscopy: The efficiency boost for QC labs
Enhance quality control in material and chemical production with NIRS. Fast, cost-effective, and no sample prep needed. Learn more in our eBook.
- EB-003EB-003Ion chromatography for food and beverage analysis
Efficiently analyze food products with ion chromatography (IC). Discover its robust applications in quality control for beverages, food additives, and dairy.
- EB-004EB-004Near-infrared and Raman spectroscopy for polymer analysis: An introduction
This e-book explains how Raman and near-infrared (NIR) spectroscopy enable rapid, nondestructive polymer analysis, ensuring high quality while reducing costs and waste.
- TA-016TA-016Determination of mercury and arsenic using speciation analysis (IC-ICP/MS)
The combination of ion chromatography and inductively coupled plasma mass spectrometry (IC-ICP/MS) is ideally suited for the detection of species of arsenic and mercury in their various oxidation levels and forms of chemical bonding. However, some species – as in the case of mercury – are reciprocally converted into one another during sample preparation, thus making a determination of the initial concentrations of the heavy metal species impossible. This article shows how these interconversions can be calculated with isotope dilution analysis and IC-ICP/MS in accordance with EPA method 6800.
- TA-019TA-019Simultaneous determination of mineral acids, fluoride and silicate in etching baths.
This article describes an ion chromatography method for the simultaneous determination of HF, HNO3, H2SO4, short-chain organic acids, and of H2SiF6 in acid texturing baths.
- TA-020TA-020IC-MS and IC-ICP/MS analysis in the environment
This article describes the coupling of ion chromatography with mass spectrometry (IC-MS) and plasma mass spectrometry (IC-ICP/MS) for the trace analysis of potentially hazardous compounds in the environment.
- TA-021TA-021Determination of the halogen and sulfur content in complex organic matrices by means of Combustion Ion Chromatography (CIC)
The automated combination of pyrolysis and subsequent ion chromatography (Combustion IC) permits the parallel detection of halogens and sulfur in all flammable solid and liquid matrices. The method is captivating, not only because of its outstanding precision and trueness, but also because of the high sample throughput.
- TA-023TA-023Investigation of MRT contrast media containing gadolinium by means of IC-ICP/MS analysis
This article describes the investigation using ion chromatography and subsequent inductively coupled plasma mass spectronomy (ICP/MS) to determine the extent to which the iron(III) flocculation carried out in the context of wastewater treatment releases toxic gadolinium(III) ions as the result of recomplexing.
- TA-044TA-044pH value, conductivity and titration in water and soil analysis
The rapid growth of the Earth's population has led to massive increases in the consumption of energy and resources and in the production of consumer products and chemicals. It is estimated that 17 million chemical compounds are currently on the market, of which 100,000 are produced on a large industrial scale. Many of these enter the environment. This leads to a demand for sensitive analytical procedures and high-performance analytical instruments.pH value, conductivity and oxygen requirement are important characteristics in water and soil analysis. The first two of these can be determined rapidly; for the third, the titration that is used is also the one used in numerous single determinations. This article describes several important standard-compliant determinations in water and soil analysis.
- TA-052TA-052IC-ICP-MS analysis of iodized X-ray contrast media
On the basis of the experiments that have been performed, it is possible to determine the effectiveness of the ozonization of iodized X-ray contrast media using IC-ICP-MS via the amount of iodate formed. Whereas a 120-minute ozonization guarantees a practically quantitative decomposition of amidotrizoic acid to iodate, approximately 16% of the Iomeprol is still present under the same ozonization conditions. Given that only 14% is present in iodate form in the absence of iodide anions and given that additional, not yet identified peaks occur in the ion chromatogram, the presence of additional decomposition products containing iodine must be assumed. Nonetheless, it is not possible to detect the intact iodized X-ray contrast media with the selected ion chromatographic conditions. Furthermore, the possibility exists of identifying the peak of the unknown decomposition product of the Iomeprol using IC-ESI-TOF-MS.
- TA-054TA-054Online monitoring of atmospheric inorganic gases and aerosols in the Southeast and Northwest of the United States
This article describes the composition of atmospheric inorganic gases and aerosols in the Southeast and Northwest of the United States during a time period of several weeks. The semicontinuous sampling in hourly cycles takes place using the MARGA system from Metrohm Applikon. The temporal resolution of the aerosol and gas composition makes it possible to generate statements regarding the chemical origin and hygroscopicity of the particles. These are fundamental for rating the influence of aerosols on the climate.
- TA-057TA-057Chromate in toys, leather and drinking water
Chromate is allergenic, carcinogenic and extremely toxic. It is therefore subject to strict monitoring. It is present in different concentrations in drinking water, toys, textiles, leather and many other materials. Metrohm has developed various methods for ion chromatographic determination of chromium(VI) which, thanks to Inline Sample Preparation, are suitable for a variety of matrices and concentration ranges – from ng/L to mg/L.
- WP-001WP-001Chromium(VI) determination in children's toys
This article describes a simple and sensitive method for chromium(VI) determination in children's toys. The solution to be analyzed is prepared in accordance with DIN EN 71. Not only VIS detection but also post-column derivatization using diphenylcarbizide are parts of this method. The procedure described here is suitable for the precise determination of hexavalent chromium in the single-digit ppt range and, in addition, fulfils without difficulty the limit value of 10 ppt prescribed by the EU directive 2009/48/EC.
- WP-002WP-002Basics of potentiometry
The present article addresses the theory, practical aspects and troubleshooting of potentiometry.
- WP-003WP-003pH measurement: Six technical tips
This white paper presents six technical tips that you should consider before taking a pH measurement.
- WP-004WP-004Electrochemistry in the environmental sciences
This Metrohm White Paper presents the important role of electrochemistry in the environmental sciences. The applications have to do with basic research for the fuel cell that yields energy from wastewater, the electrical clean-up of contaminated soil and electrochemical CO2 reduction of greenhouse gases for isolating chemical raw materials.
- WP-007WP-007Electrochemistry in the quality control of food packaging
The shelf life of foods and beverages depends among other things on the packaging material used. Metals are ideally suitable for packaging, as they can be laminated with various passivating and food-compatible layers. Electrochemical measurements such as Electrochemical Impedance Spectroscopy (EIS) make it possible to check the layers for damage.
- WP-008WP-008Coupling of ion chromatography and plasma mass spectrometry
The coupling of ion chromatography and inductively coupled plasma mass spectrometry (ICP/MS) leads to a high-performance measurement system that masters several particularly challenging analyses. It enables for example reliable determination of element compositions, oxidation states and chemical bonds. This information is used, for example, for assessing the toxicity of medications, environmental and water samples as well as foods and beverages.
- WP-009WP-009Determination of anions in tap water in accordance with US EPA Method 300
This article describes a simple method for the determination of seven standard anions (fluoride, chloride, nitrite, bromide, nitrate, phosphate and sulfate) in accordance with US EPA Method 300 Part A. An IC system is extended to include Inline Ultrafiltration and Inline Eluent Preparation for the analysis.
- WP-010WP-010Glyphosate and AMPA in drinking water
For the first time, glyphosate determination and that of its primary metabolite AMPA in drinking water using IC with pulsed amperometric detection (flexIPAD) in the low µg/L range are shown. Compared to HPLC analysis with a mass-selective detector, it is a very cost-effective method for determining the glyphosate and AMPA content in water and foodstuffs. With a detection limit at approx. 1 µg/L, compliance with limit values for glyphosate can be monitored in the USA, Canada, and Australia, among others.
- WP-011WP-011Sustainable Testing of Paint and Coatings
More strict regulations paired with more complex products have increased testing complexity in the paint and coating industry. Therefore, producers ask for more powerful, safe and sustainable analytical methods. Testing by Vis-NIR spectroscopy is a sustainable and costefficient alternative to many wet chemical methods. This white paper describes how Vis-NIR spectroscopy improves testing procedures for various analyses during the formulation and production of paint and coatings in an economic and ecological way.Key words: testing, sustainable, VOC, paint, coating, binders, resins, additives, pigments, solvents
- WP-012WP-012Corrosion control: Thermometric TAN analysis in oil & refinery distillation fractions
Many refiners look at discounted opportunity crudes as a means to improve their margin spread. The varieties of these cheap crude oils on the market are growing in number, but they have hidden risks for the purchaser caused by factors such as high naphthenic acid and sulfur content. Sulfur compounds and naphthenic acids are among the substances that contribute to the corrosive nature of crude oils and petroleum products. This is why the risk of corrosion is increased when processing crude oils with high naphthenic acid and sulfur content. The refiner must balance the cost benefit versus the risk and the cost of corrosion control when processing these crudes. A reliable acid number determination is a crucial part of corrosion control. Guest authors Bert Thakkar, Bryce McGarvey, and Colette McGarvey of Imperial Oil and Larry Tucker and Lori Carey of Metrohm USA were involved in the development of the new ASTM Method D8045 for acid number determination. Here, they report on the method and how it came to be.
- WP-014WP-014High productivity and profitability in IC environmental analysis
Brad Meadows is Vice President and Lab Director at the US company BSK Labs, which runs a number of environmental laboratories and service centers. Brad is an analytical chemist and has been working in the management of analysis laboratories for 15 years. He shared his experiences with Metrohm ion chromatography with us in the form of some concrete facts and figures.
- WP-017WP-017Near-infrared spectroscopy in pharmacopoeias
The pharmaceutical industry is very likely more comprehensively regulated that any other branch of industry. It therefore requires analytic methods that meet the requirements of regulations while at the same time being practical. This applies in particular for large sample quantities, such as are encountered with incoming goods inspections, for example. It is here that particularly rapid and simple analysis methods are called for which make routine analyses simpler and more efficient. This White Paper describes some of the most important regulations in the pharmaceutical analysis and shows how Vis-NIR spectroscopy can solve analytic problems in the pharmaceutical industry in accordance with regulations.
- WP-018WP-018FDA 21 CFR Part 11 Requirements for NIR Spectroscopy
This Metrohm White Paper shows the requirements demanded of the pharmaceutical industry by the FDA with respect to software products. Implementation examples of the regulations formulated by the FDA in 21 CFR Part 11 are presented using Vision Air Pharma Software.Key words: electronic signatures, audit trails, user management, documentation
- WP-019WP-019Ion chromatography – a universal technique with many applications in the pharmaceutical industry
Ion chromatography is a flexible technique with a large selection of intended uses in the pharmaceutical industry. – A few development trends and the latest advances are displayed here.
- WP-020WP-020Near-infrared spectroscopy: Technology comparison
This White Paper compares the two most commonly used technologies in near-infrared spectroscopy: Predispersive monochromator technology and Fourier transformation technology. In addition to measurement speeds and captured spectral ranges, the noise levels and the signal-noise ratios associated with them are also contrasted with one another.
- WP-021WP-021Water analysis in the field: Determining arsenic, mercury, and copper
Heavy metals such as arsenic and mercury find their way into the ground water in many regions of the world, either through natural processes or as the result of human activities. Limit values are exceeded many times over, particularly for arsenic in drinking water, in many areas. This calls for a rigorous monitoring of water quality. The present whitepaper focuses on field determinations of arsenic, mercury, and copper – directly at the sampling site.
- WP-022WP-022In situ SERS effect with screen-printed silver electrodes
In this work, time resolved Raman spectroelectrochemistry measurements with screen printed electrodes are shown. The instrument used combines in a totally integrated box: a 785 nm laser source, a high resolution Raman spectrometer and a bipotentiostat/galvanostat. Experiments are controlled with an excellent spectroelectrochemical software which allows real time data collection and useful data treatment.
- WP-023WP-023Karl Fischer titration and near-infrared spectroscopy in perfect synergy
Metrohm has shaped moisture analysis for more than half a century. Find out about new developments in water analysis and learn how near-infrared spectroscopy in combination with Karl Fischer titration can increase your sample throughput and boost your productivity.
- WP-024WP-024Verification, p-values, and Training Sets for the Mira P
This white paper differentiates between methods for identification of unknowns and verification of known materials. The goal of this publication is, ultimately, to inform the user of the capabilities of the handheld Metrohm Raman Mira P system. Best practices for building robust training sets for materials verification with Mira P can also be found here.
- WP-026WP-026Surface Enhanced Raman Scattering (SERS) – Expanding the Limits of Conventional Raman Analysis
Surface Enhanced Raman Scattering or SERS is an anomalous enhancement of Raman scattering when molecules are adsorbed to gold or silver nanoparticles – this enhancement can be as large as 107. The advantage of SERS for the analytical chemist lies in its ability to detect analyte concentrations of parts per million and even parts per billion levels, while classical Raman is limited to parts per thousand. Metrohm Raman produces P-SERS assays in the form of nanoparticles printed onto substrates using inkjet technology. This method produces inexpensive test strips that exhibit exceptional stability and sensitivity. There are two markets that can be easily addressed with P-SERS: forensic analysisand food safety. This white paper explains the mechanism of SERS and how it can be applied to handheld Raman analysis with Metrohm Raman Mira systems.
- WP-027WP-027Smart Acquire – Automated Raman Material ID for Defense and Security Professionals
An analytic chemist in your back pocket. A forensic laboratory in a suitcase. A HazMat team in the trunk of your car. First responders need all the help they can get when faced with potentially dangerous substances. Mira DS from Metrohm Raman is a sophisticated chemical analyzer that replaces the specialist with automation. The push of a button initiates proprietary Smart Acquire routines to optimize acquisition parameters and collect the highest quality spectra. These spectra are automatically subjected to library search and Mixture Matching routines capable of identifying up to three components of a mixture. When hazardous substances are detected, the user is alerted to immediate action with color-coded warnings.
- WP-028WP-028Safety in Any Situation – Addressing the needs of first responders
Metrohm Raman presents a unique handheld materials identification system designed to meet the needs of defense and security professionals. Meet Mira DS, the most adaptable Raman analyzer available today. Mira DS was developed directly in response to requests from first responders in the field for a small, rugged, automated materialsidentification system that ensures the safety of the user in any situation.
- WP-029WP-029Near-Infrared Spectroscopy: Quantitative analysis according to ASTM E1655
Near-Infrared spectroscopy (NIRS) is a widely used analytical technique for quantitative analysis of various products in research and industrial applications. This white paper summarizes the workflow of the development of quantitative methods according to ASTM E1655.
- WP-030WP-030Analytical method transfer
Near-infrared spectroscopy (NIRS) is a widely used analytical technique for qualitative and quantitative analysis of various products in research and industrial applications. Because of different reasons it might be necessary to transfer analytical methods from one NIR analyzer to another one. This white paper summarizes the workflow of such method transfer.
- WP-031WP-031Lifecycle of multivariate methods according to United States Pharmacopeia Chapter <1039> Chemometrics
Chemometrics is a powerful tool widely used for method development in the pharmaceutical industry. This whitepaper describes the lifecycle of multivariate models and summarizes the workflow of the development of chemometrical models according to the new USP chapter <1039>.
- WP-032WP-032Creating Custom Libraries Detection of Binary Explosives with Mira DS
Detection of threatening materials requires robust and sophisticated instruments capable of safe, instantaneous field-analysis of unknowns. In an environment where there is an ever-evolving threat of explosives made from commonlyavailable chemicals, explosive libraries must be customized constantly to include newly targeted materials. Mira DS from Metrohm Raman is the perfect solution for detection of explosives in the field. This handheld Raman instrument is equipped with sophisticated analysis algorithms and a suite of safety features for first responders who need the identity of a potential hazard... NOW! Mira DS and its software can be customized to respond to emerging hazards: this note describes procedures for creating custom libraries of binary explosive precursors to be used in library comparison and mixture matching routines on Mira DS. With these tools, unknown substances can be identified with color-coded warnings for fast action in critical situations.
- WP-033WP-033Identifying Narcotics in Complex Samples
A person suspected of possessing a narcotic can be charged with a crime only after the identity of the illicit substanceis confirmed. This confirmation is typically provided by analytical chemists in forensic laboratories and requires highly technical separation and detection methods. Unfortunately, such labs often have deep caseloads that lead to delays in testing. Handheld Raman analyzers bring the reliability and accuracy of lab analysis to first responders in the field, allowing for rapid and accurate identification of street drugs with a white powder appearance. With such tools, demand for forensic analysis can be reduced and enforcement agencies can enforce drug policies with greater safety, speed, and precision.
- WP-034WP-034Determination of Heroin in Street Drug Samples
Printable Surface Enhanced Raman Scattering (P-SERS) silver substrates were used with Metrohm Raman’s Mira DS handheld Raman analyzer to successfully detect heroin in 18 crude street heroin samples. Detection of heroin with P-SERS was accomplished easily and very quickly, with minimal sample clean-up. Solvent studies were also implemented to determine the optimal solvent for crude sample extraction, with results included here.
- WP-035WP-035Facile Verification of Edible Oils with Raman Spectroscopy
Edible oils comprise a significant portion of any diet, and they also have important roles in the production of foods, cosmetics, and skincare products. For these reasons, a convenient and accurate method for materials identification of a variety of fats and oils is highly desirable. Historically, authentication of fats and oils was performed through intensive laboratory techniques involving chromatographic methods. Here, Raman spectroscopy combined with Principle Component Analysis (PCA) has been used for materials identification with 16 different edible oils, with excellent results. Raman is an ideal technique for evaluation of fats, as carboncarbon double- and single-bonds give strong Raman signals. PCA analysis in combination with Raman spectroscopy is a powerful tool for qualification and verification of different fats and oils, as there are few visual differences between spectra of edible oils.
- WP-036WP-036Lean manufacturing of polyurethane, assisted by near-infrared (NIR) and Raman spectroscopy
Chemical manufacturing such as polyurethane production is characterized by a cost intensive production process combined with a negative ecological impact. These adverse effects can be significantly improved by using vibrational spectroscopy. This analytical technique can assist the operator of the plant to reduce costs and minimize the impact onthe environment as is demonstrated in the present white paper.
- WP-037WP-037Simplifying quality control using Near-Infrared Spectroscopy
Quality control is impacted by multiple challenges, which can have an influence on the functioning of the QC lab. The present White Paper provides approaches, how to simplify the daily quality control using near-infrared spectroscopy combined with a dedicated smart software like Vision Air.
6.5703.010
Consumable Kit ICAssembly of important expendable items for ion chromatography.
6.5703.020
Consumable Kit CVSAssembly of important expendable items for CVS applications with Professional CVS instruments.
6.5706.010
Consumable Kit Biodiesel RancimatAssembly of important expendable items for the Biodiesel Rancimat.
6.5706.020
Consumable Kit RancimatAssembly of important expendable items for the Rancimat.
6.5865.600
Initial inst. Kit, ceramic combustion tube AJInitial installation kit of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ). Contains the suitable heat guard for the usage of the ceramic combustion tube CIC AJ.
6.5904.030
Rotor, 6/2 injectorRotor for the 6/2 injector in IC systems.
6.5904.050
Injector with 0.25 µL internal loopFlat plate injector with 0.25 µL internal loop
6.5904.060
Rotor (internal loop, 0.25 µL)Rotor for 4-port flat plate injector (6.5904.050), 0.25 µL internal loop
6.5904.070
Rotor (internal loop, 1.0 µL)Rotor for 4-port flat plate injector (6.9956.001), 1.0 µL internal loop
6.5904.210
Stator, 6/2 injectorStator for the 6/2 injector in IC systems.
6.5904.220
Stator for MF internal loop injectorStator for 4-port valve (internal loop injector, 6.5904.050 and 6.9959.001),
6.7301.180
Finger-Tight-Set 1/8 in.Finger-Tight for gas connection on the Automatic Boat Driver
6.7301.200
Guide tubing for ABD (new)Guide tubing for Automatic Boat Driver of the Combustion Module (ABD serial numbers starting with 1709591)
6.7301.270
Pin wrench, 2 mm, adjustable to ABDThe wrench is used for assembly/disassembly of the combustion tube in the ABD.
6.7301.280
Cover hood for ABD/MMS 5000Cover hood for protecting the samples on the ABD/MMS 5000 against contamination.
6.7301.300
Ceramic combustion tube CIC AJ, completeCeramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7301.310
Outer tube, ceramic combustion tube AJOuter tube of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7301.320
Connecting tube, ceramic combustion tube AJConnecting tube of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7301.330
Ceramic inlay, ceramic combustion tube AJCeramic inlay of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7301.340
Frit, ceramic combustion tube AJFrit of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7301.350
Clamping screw, ceramic combustion tube AJClamping screw of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7301.360
Union nut, ceramic combustion tube AJUnion nut of the ceramic combustion tube for the Combustion Module (Oven + ABD, AJ).
6.7302.000
Kit for solid samples for MMS 5000, 35 positionsKit for solid samples for MMS 5000 with rack for sample boats, grippers and 10 quartz glass boats.
6.7302.200
Gripper for boatGripper for solid changer setup MMS 5000
6.7302.300
Boat sensor for ABDBoat sensor for ABD in the Combustion IC system.
6.7302.310
Sample rack 35 positions for solid samplesFor solids.
6.7303.000
Kit for liquid samples for MMS 5000, 112 positionsKit for liquid samples for MMS 5000 with rack for sample vessels, 100 µL syringe with replaceable needle and 100 snap-ring bottles.
6.7303.300
CIC Liquid Sampler solvent reservoirReservoir for rinsing the sample needle on the Autosampler MMS 5000 with liquids kit.
6.7303.310
Sample rack 112 positions for liquid samplesFor liquid samples.
6.7304.020
Oxygen/argon connection tubing, 2 mConnection tubing for gas supply for the Combustion Module
6.7304.030
Oven coupling for LPG/GSS (AJ)Connector for connecting the LPG/GSS module (AJ) to the combustion oven. For Metrohm Combustion IC.
6.7305.000
Blower vesselBlower vessel for LPG/GSS Module.
6.7305.010
Screw connector, complete, for blower vessel.Screw connector for fastening to the blower vessel.
6.7305.050
T-connector to LPG/GSS ModuleT-connector with two 6/4 mm, 10 cm and 70 cm connection tubings
6.7400.000
NIRS XDS accessory kitAccessory kit for NIRS XDS laboratory monochromators
6.7400.010
NIRS Liquid Sample Kit TransflectionThe NIRS Liquid Sample Kit Transflection supplements the following instruments with the function of the transflection measurement of liquids:NIRS DS2500 Analyzer (order number: 2.922.0010); NIRS XDS MasterLab Analyzer (order number: 2.921.1310); NIRS XDS MultiVial Analyzer (order number: 2.921.1120); NIRS XDS RapidContent Analyzer (order number: 2.921.1110); NIRS XDS RapidContent Analyzer - Solids (order number: 2.921.1210);
6.7400.030
NIRS DS2500 accessory kitAccessory kit for NIRS DS2500 Analyzer
6.7401.000
NIRS transflection vessel, optically flatOptically flat transflection vessel for the spectral measurement of liquids. Can be used in combination with the following instruments:NIRS DS2500 Analyzer (order number: 2.922.0010); NIRS XDS MasterLab Analyzer (order number: 2.921.1310); NIRS XDS MultiVial Analyzer (order number: 2.921.1120); NIRS XDS RapidContent Analyzer (order number: 2.921.1110); NIRS XDS RapidContent Analyzer - Solids (order number: 2.921.1210);
6.7401.040
NIRS XDS quartz cuvette, screw top, 20 mm pathlengthQuartz cuvette, screw top, with 20 mm pathlength for the recording of a spectrum of volatile liquids in transmission using an NIRS XDS RLA Analyzer.
6.7401.110
NIRS XDS quartz cuvette with open top, 0.5 mm pathlengthOpen quartz cuvette with 0.5 mm pathlength for the recording of a spectrum of liquids in transmission using an NIRS XDS RLA Analyzer.
6.7401.200
Quartz cuvette, 1 mmQuartz glass cuvette with a window made of quartz glass of maximum purity and homogeneity. The cuvettes have a transmission of more than 80% in the wavelength range of 200–2500 nm.Compatible with:NIRS Spacer for set of 12.5 mm cuvettes (6.7403.180); DS2500 holder for 1 mm cuvette (6.7492.100); Holder OMNIS NIR, cuvette, 1 mm (6.07401.010);
6.7401.210
Quartz cuvette, 2 mmQuartz glass cuvette with a window made of quartz glass of maximum purity and homogeneity. The cuvettes have a transmission of more than 80% in the wavelength range of 200–2,500 nm.Compatible with:NIRS Spacer for set of 12.5 mm cuvettes (6.7403.180); DS2500 holder for 2 mm cuvette (6.7492.110); Holder OMNIS NIR, cuvette, 1 mm (6.07401.010) ;
6.7401.220
Quartz cuvette, 5 mmQuartz glass cuvette with a window made of quartz glass of maximum purity and homogeneity. The cuvettes have a transmission of more than 80% in the wavelength range of 200–2500 nm.Compatible with:NIRS Spacer for set of 12.5 mm cuvettes (6.7403.180); DS2500 holder for 5 mm cuvette (6.7492.120); Holder OMNIS NIR, cuvette, 5 mm (6.07401.030);
6.7401.230
Quarzküvette, 10 mmQuarzglasküvette mit einem Fenster aus Quarzglas in höchster Reinheit und Homogenität. Die Küvetten haben eine Transmission von über 80% im Wellenlängenbereich von 200 nm - 2500 nm.Kompatibel mit:NIRS Spacer für 12.5 mm Küvettenset (6.7403.180); DS2500 Halter für 10 mm Küvette (6.7492.130); Halter OMNIS NIR, Küvette, 10 mm (6.07401.040) ;
6.7401.300
Flow-through cell, 0.5 mmFlow quartz cuvettes with quartz glass window and an optical path length of 0.5 mm suitable for near-infrared spectroscopy (NIRS) analyses.Compatible with:Holder OMNIS NIR, flow-through cell (6.070401.100); DS2500 holder for flow cells (6.7493.000);
6.7401.310
Flow-through cell, 1 mmFlow quartz cuvettes with an optical path length of 1.0 mm suitable for near-infrared spectroscopy (NIRS) analyses.Compatible with:Holder OMNIS NIR, flow-through cell (6.07401.100); DS2500 holder for flow cells (6.7493.000) ;
6.7401.320
NIRS 12.5 mm quartz cuvette flow 2 mmThe flow quartz cuvettes enable continuous monitoring, for example of tablet disintegration processes and reaction kinetics. The high pressure resistance and a special bubble capturing system make all measurements particularly easy.Windows made of quartz glass of maximum purity and homogeneity ensure a transmission of more than 80% in the wavelength range of 200 nm - 2,500 nm.A variety of pathlengths are available:0.5 mm pathlength and a volume = 175 μL (order number: 67401300)1 mm pathlength and a volume = 350 μL (order number: 67401310)2 mm pathlength and a volume = 700 μL (order number: 67401320)5 mm pathlength and a volume = 1,750 μL (order number: 67401330)10 mm pathlength and a volume = 3,500 μL (order number: 67401340)Dimensions h x l x w = 35 mm x 12.5 mm x 12.5 mmWindow height = 8.5 - 15 mmCompatible with the NIRS spacer for the XDS RapidLiquid Analyzer and the DS2500 holder for the DS2500 Liquid Analyzer.
6.7401.330
NIRS 12.5 mm quartz cuvette flow 5 mmThe flow quartz cuvettes enable continuous monitoring, for example of tablet disintegration processes and reaction kinetics. The high pressure resistance and a special bubble capturing system make all measurements particularly easy.Windows made of quartz glass of maximum purity and homogeneity ensure a transmission of more than 80% in the wavelength range of 200 nm - 2,500 nm.A variety of pathlengths are available:0.5 mm pathlength and a volume = 175 μL (order number: 67401300)1 mm pathlength and a volume = 350 μL (order number: 67401310)2 mm pathlength and a volume = 700 μL (order number: 67401320)5 mm pathlength and a volume = 1,750 μL (order number: 67401330)10 mm pathlength and a volume = 3,500 μL (order number: 67401340)Dimensions h x l x w = 35 mm x 12.5 mm x 12.5 mmWindow height = 15 mmCompatible with the NIRS spacer for the XDS RapidLiquid Analyzer
6.7401.340
NIRS 12.5 mm quartz cuvette flow 10 mmThe flow quartz cuvettes enable continuous monitoring, for example of tablet disintegration processes and reaction kinetics. The high pressure resistance and a special bubble capturing system make all measurements particularly easy.Windows made of quartz glass of maximum purity and homogeneity ensure a transmission of more than 80% in the wavelength range of 200 nm - 2,500 nm.A variety of pathlengths are available:0.5 mm pathlength and a volume = 175 μL (order number: 67401300)1 mm pathlength and a volume = 350 μL (order number: 67401310)2 mm pathlength and a volume = 700 μL (order number: 67401320)5 mm pathlength and a volume = 1,750 μL (order number: 67401330)10 mm pathlength and a volume = 3,500 μL (order number: 67401340)Dimensions h x l x w = 35 mm x 12.5 mm x 12.5 mmWindow height = 15 mmCompatible with the NIRS spacer for the XDS RapidLiquid Analyzer
6.7402.020
NIRS disposable backs for 6.7402.030, 100 pcs.The disposable backs are used for the secure sealing of the mini sample cups. The sample cups are used in the following:NIRS DS2500 Analyzer (order number: 2.922.0010); NIRS XDS MasterLab Analyzer (order number: 2.921.1310); NIRS XDS RCA Analyzer (order number: 2.921.1110); NIRS XDS MultiVial Analyzer (order number: 2.921.1210); The package is comprised of 100 disposable backs.
6.7402.030
NIRS mini sample cups, 10 pcs. including 100 disposable backsMini sample cup for the spectral recording of powders and granulates in reflection. The sample cup can be sealed with disposable backs in order to avoid sample loss and for the uniform distribution of the powder or granulate in the sample cup.The sample cups are used with the following instruments:NIRS DS2500 Analyzer (order number: 2.922.0010); NIRS XDS MasterLab Analyzer (order number: 2.921.1310); NIRS XDS MultiVial Analyzer (order number: 2.921.1120); NIRS XDS RapidContent Analyzer (order number: 2.921.1110); NIRS XDS RapidContent Analyzer - Solids (order number: 2.921.1210);
6.7402.040
NIRS XDS coarse granular sample cellNIRS XDS coarse granular sample cell for the reflection measurement of samples with different surface properties.
6.7402.050
DS2500 large sample cupLarge sample cup for the spectral recording of powders and granulates in reflection at various sample positions using the NIRS DS2500 Analyzer.
6.7402.060
NIRS DS2500 large sample cup, 5 pcs.Set of five large sample cups for the spectral measurement of powders and granulates in reflection using the NIRS DS2500 Analyzer.
6.7402.070
Disposable vials, 2 mm diameter, transmission200 lockable disposable glass vials (borosilicate) with a diameter of 2 mm for analyses of liquids in transmission mode.Compatible with:Holder OMNIS NIR, vial, 2 mm (6.07401.050); DS2500 holder for flow cells (6.7492.000);
6.7402.100
Disposable vials, 10 mm diameter, transmission195 lockable disposable glass vials (borosilicate) with a diameter of 10 mm for analyses of liquids in transmission.Compatible with:Holder OMNIS NIR, vial, 10 mm (6.07401.080); DS2500 holder for 4 mm disposable vials (6.7492.030);
6.7402.110
Disposable vials, 15 mm, reflection123 lockable disposable glass vials with a diameter of 15 mm for analyses of solids in reflection. Suitable for NIRS RapidContent (Solid) Analyzers of the XDS, DS2500 and OMNIS product families.
6.7402.120
Disposable vials, 19 mm, reflection225 lockable disposable glass vials with a diameter of 19 mm for analyses of solids in reflection. Suitable for NIRS RapidContent (Solid) Analyzers of the XDS, DS2500 and OMNIS product families.
6.7402.130
Disposable vials, 22 mm, reflection172 lockable disposable glass vials with a diameter of 22 mm for analyses of solids in reflection. Suitable for NIRS RapidContent (Solid) Analyzers of the XDS, DS2500 and OMNIS product families.
6.7402.140
Disposable vials, 28 mm, reflection216 lockable disposable glass vials with a diameter of 28 mm for analyses of solids in reflection. Suitable for the following analyzers:NIRS DS2500 Analyzer; NIRS XDS RapidContent (Solid) Analyzer; NIRS XDS MultiVial Analyzer; NIRS XDS MasterLab Analyzer;
6.7402.150
DS2500 lid for large sample cupLid for the large sample vessel for the DS2500 Analyzer.
6.7402.200
Stopper for 6.7402.110123 stoppers for 15 mm Reflection disposable vials.
6.7402.210
Stopper for 6.7402.120225 stoppers for 19 mm Reflection disposable vials.
6.7402.220
Stopper for 6.7402.130172 stoppers for 22 mm Reflection disposable vials.
6.7402.230
Stopper for 6.7402.140216 stoppers for 28 mm Reflection disposable vials.
6.7402.240
Disposable vial, 8 mm, transmission, qty. 100100 disposable glass vials (borosilicate) with an optical path length of 8 mm for analyses of liquids in transmission. The disposable vials are supplied with the associated stoppers (number of pieces = 100).Compatible with:Holder OMNIS NIR, vial, 8 mm (6.07401.070); DS2500 holder for 8 mm disposable vials (6.7492.020) ;
6.7402.250
Disposable vial, 4 mm, transmission, qty. 200200 disposable glass vials (borosilicate) with an optical path length of 4 mm for analyses of liquids in transmission. Compatible with:Holder OMNIS NIR, vial, 4 mm (6.07401.060); DS2500 holder for 4 mm disposable vials (6.7492.010);
6.7402.260
Stopper for disposable vial, 4 mm, qty. 100100 stoppers for 4 mm transmission disposable vials (6.7402.250).
6.7403.000
NIRS XDS spacer for disposable 8 mm vials (6.7402.000)Spacer for disposable glass vials with 8 mm diameter.
6.7403.010
NIRS XDS spacer for disposable 4 mm vials (6.7402.010)Spacer for disposable glass vials with 4 mm diameter
6.7403.020
XDS spacer for disposable 2 mm vials (6.7402.070)Spacer for the disposable glass vials with 2 mm diameter.
6.7403.030
XDS spacer for disposable 10 mm vials (6.7402.100)Spacer for the disposable glass vials with 10 mm diameter.
6.7403.110
NIRS XDS spacer for 0.5 mm cuvettes (6.7401.110)Spacer for fixing open quartz cuvettes with 0.5 mm total pathlength in an NIRS XDS RLA Analyzer.
6.7403.180
NIRS Spacer for 12.5 mm cuvettesThe NIRS Spacer for 12.5 mm cuvette set ensures spacers for an optimum position of the cuvette in the sample holder.
6.7404.000
Aperture plateAperture plate for reducing the spot size to 4.5 mm, in particular for analyzing tablets with the aid of the XDS MasterLab Analyzer.
6.7410.000
NIRS XDS tray for reflection standardA reflection standard is required for the calibration of the monochromator with the sample module. A holder in which the standard is positioned is used to fasten the calibration standard in place. A reflection standard and its associated holder are required for:NIRS XDS MultiVial Analyzer (order number: 29211210); NIRS XDS MasterLab Analyzer (order number: 2.921.1310);
6.7410.010
NIRS MultiVial tray for 4x5 15 mm vialsNIRS MultiVial tray for 4x5 15 mm vials
6.7410.020
NIRS MultiVial tray for 3x5 19 mm vialsNIRS MultiVial tray for 3x5 19 mm vials
6.7410.030
NIRS MultiVial tray for 3x5 22 mm vialsNIRS MultiVial tray for 3x5 22 mm vials
6.7410.040
NIRS MultiVial tray for 2x3 27 mm vialsNIRS MultiVial tray for 2x3 27 mm vials
6.7410.050
NIRS MultiVial tray for 2x3 29 mm vialsNIRS MultiVial tray for 2x3 29 mm vials
6.7410.090
NIRS tablet tray for different tablet shapesNIRS tablet tray for different tablet shapes
6.7410.110
NIRS FlexiTrayThe NIRS FlexiTray permits maximum flexibility when analyzing tablets and capsules. A variety of forms are reproducibly positioned with the aid of the spring mechanism in order to ensure accurate and precise measurement results at all times.
6.7420.000
NIRS gold diffuse reflector, 1 mm total pathlengthGold diffuse reflector for the transflection measurement of liquids. Can be used in combination with the following instruments:NIRS DS2500 Analyzer (order number: 2.922.0010); NIRS XDS MasterLab Analyzer (order number: 2.921.1310); NIRS XDS MultiVial Analyzer (order number: 2.921.1120); NIRS XDS RapidContent Analyzer (order number: 2.921.1110); NIRS XDS RapidContent Analyzer - Solids (order number: 2.921.1210);
6.7420.010
NIRS gold diffuse reflector, 2 mm total pathlengthGold diffuse reflector for the transflection measurement of liquids. Can be used in combination with the following instruments:NIRS DS2500 Analyzer (order number: 2.922.0010); NIRS XDS MasterLab Analyzer (order number: 2.921.1310); NIRS XDS MultiVial Analyzer (order number: 2.921.1120); NIRS XDS RapidContent Analyzer (order number: 2.921.1110); NIRS XDS RapidContent Analyzer - Solids (order number: 2.921.1210);
6.7420.020
NIRS gold diffuse reflector, 4 mm total pathlengthGold diffuse reflector for the transflection measurement of liquids. Can be used in combination with the following instruments:NIRS DS2500 Analyzer (order number: 2.922.0010) NIRS XDS MasterLab Analyzer (order number: 2.921.1310) NIRS XDS MultiVial Analyzer (order number: 2.921.1120) NIRS XDS RapidContent Analyzer (order number: 2.921.1110) NIRS XDS RapidContent Analyzer - Solids (order number: 2.921.1210)
6.7425.000
NIRS XDS irisIris for focusing mini sample vessels, reflection standard, various vials or a transflection vessel in the NIRS XDS RCA Analyzer, the NIRS XDS MasterLab Analyzer and the NIRS XDS MultiVial Analyzer
6.7425.100
DS2500 IrisThe iris for the DS2500 with a variably adjustable diameter of up to 36 mm enables you to perform flexible reflection measurement investigations of samples in vials.The iris for the DS2500 is used in the holder for small sample vessels. Order number: 6.7430.040
6.7430.000
NIRS XDS lab spare lampSpare lamp with 12 V and 50 W for the monochromator of the NIRS XDS laboratory instruments
6.7430.010
NIRS XDS lab spare parts kitNIRS XDS spare parts kit of the lab instrument is comprised of two spare lamps, two fan filters and four fuses.
6.7430.030
NIRS transmission pair calibration fixtureNIRS transmission pair calibration fixture
6.7430.040
DS2500 HolderHolder for use with:Small sample vessels (6.7402.030); DS2500 Iris (6.7425.100);
6.7430.050
Spare lamp for NIRS DS2500Spare lamp with 12.0 V and 35 W for NIRS DS2500 Analyzer
6.7430.060
Micro Fiber Cleaning ClothCleaning cloth for monitors and optics.
6.7430.080
XDS Interchangeable Probe SetThe interchangeable probe set consists of a reflection probe, a transflection probe and various spacers, including fixing screws for setting variable path lengths (2 cm, 4 cm, 5 cm, and 10 cm). A protective sleeve for the probes, an Allen wrench, and a sealing ring are also included with the set.This set is part of the XDS SmartProbe Analyzer and the XDS Interactance Optiprobe Analyzer.
6.7440.170
NIRS SingleFiber optical fiber, 2 mOne-channel optical fiber in 2 m length for NIRS Process Analyzers
6.7440.480
NIRS Process, I/O Communication boxI/O Communication box for process instruments with 24 analog and 24 digital channels
6.7440.580
Transmission standard for MasterLabTransmission reference for the calibration of the XDS MasterLab for transmission measurements.
6.7450.000
NIRS reflection standard, set of 2Set of wavelength standard and 80% reflection standard for the calibration of an NIRS XDS MasterLab Analyzer, NIRS XDS RCA Analyzer, NIRS XDS MultiVial Analyzer, NIRS XDS SmartProbe Analyzer, NIRS XDS Interactance OptiProbe Analyzer and NIRS DS2500 Analyzer.
6.7450.010
NIRS reflection standard, set of 7Set comprised of six reflection standards and one wavelength standard for the calibration of an NIRS XDS MasterLab Analyzer, NIRS XDS RCA Analyzer, NIRS XDS MultiVial Analyzer, NIRS XDS SmartProbe Analyzer, NIRS XDS Interactance OptiProbe Analyzer and NIRS DS2500 Analyzer in regulated environments.
6.7450.020
NIRS tablet transmission standardNIRS transmission standard for the spectral measurement of tablets in the NIRS XDS MasterLab Analyzer
6.7450.030
Certified NIRS 99% reflection standard for laboratory sensorsCertified 99% reflection standard for calibration of an NIRS XDS SmartProbe Analyzer
6.7450.040
NIRS transmission wavelength calibration standardTransmission wavelength calibration standard for NIRS XDS RLA Analyzer and NIRS XDS Transmission OptiProbe Analyzer
6.7450.060
NIRS transmission wavelength verification standardNIRS transmission wavelength verification standard for NIRS XDS RLA Analyzer and NIRS XDS Transmission OptiProbe Analyzer
6.7450.070
NIRS 99% reflection and wavelength standard process, 1 inch diameterNIRS 99% reflection and wavelength standard for process instrument with 1 inch probe diameter
6.7450.080
NIRS 99% reflection and wavelength standard for process instrument, 0.5 inch probe diameterNIRS 99% reflection and wavelength standard for process instrument, 0.5 inch probe diameter
6.7450.090
NIRS 99% reflection and wavelength standard for process instrument, 1 inch diameter, 45° bevelNIRS 99% reflection and wavelength standard for process instrument with 1 inch diameter and 45° angle
6.7450.130
Certified wavelength and transmission standards (6-pc. set).Certified wavelength and transmission standards (0.25 AU, 0.5 AU, 1 AU, 1.5 AU and 2.0 AU) for NIRS XDS RapidLiquid Analyzer and NIRS XDS Transmission OptiProbe Analyzer in regulated environments.
6.7490.430
DS2500 Slurry CupThe Slurry Cup is the ideal sample cup for analyzing high-viscosity substances with the DS2500. The positioning of pastes and creams in the Slurry Cup is made simple by its open design, which also permits rapid and effective cleaning.In combination with the Liquid Kit (6.7400.010), clear viscous samples can also be investigated.
6.7490.440
DS2500 MultiSample Cup 15 mmDS2500 MultiSample Cup for nine 15 mm vials.
6.7490.450
DS2500 MultiSample Cup 19 mmDS2500 MultiSample Cup for eight 19 mm vials.
6.7490.460
DS2500 MultiSample Cup 22 mmDS2500 MultiSample Cup for seven 22 mm vials.
6.7490.470
DS2500 MultiSample Cup 28 mmDS2500 MultiSample Cup for six 28 mm vials.
6.7490.480
Lid for large sample cup (black)Lid (black) for the large sample cup for the DS2500 Analyzer.
6.7492.000
DS2500 Holder 2 mm vialsIntelligent holder for disposable glass vials with 2 mm diameter
6.7492.010
DS2500 Holder 4 mm vialsIntelligent holder for disposable glass vials with 4 mm diameter
6.7492.020
DS2500 Holder 8 mm vialsIntelligent holder for disposable glass vials with 8 mm diameter
6.7492.030
DS2500 Holder 10 mm vialsIntelligent holder for disposable glass vials with 10 mm diameter
6.7492.100
DS2500 Holder 1 mm cuvettesIntelligent holder for 12.5 mm cuvettes with a path length of 1 mm
6.7492.110
DS2500 Holder 2 mm cuvettesIntelligent holder for 12.5 mm cuvettes with a path length of 2 mm
6.7492.120
DS2500 Holder 5 mm cuvettesIntelligent holder for 12.5 mm cuvettes with a path length of 5 mm
6.7492.130
DS2500 Holder 10 mm cuvettesIntelligent holder for 12.5 mm cuvettes with a path length of 10 mm
6.7493.000
DS2500 Holder Flow CellIntelligent holder for 12.5 mm flow cells
6.7494.000
DS2500 Liquid Wavelength Calibration StandardIntelligent transmission wavelength calibration standard for the DS2500 Liquid Analyzer
6.7494.500
DS2500 Liquid Analyzer Heat ProtectionDS2500 Liquid Analyzer Heat Protection as optional protection for analysis at high temperatures.
6.7502.000
Glass vials for Mira M-1 Basic and Advanced PackageGlass vials suitable for use with Mira M-1 Basic and Advanced Package.
6.7502.010
Glass Vials for MIRA, 144 piecesGlass vials for use with MIRA systems. 15 mm x 26 mm.144 glass vials are included in the scope of delivery.
6.7502.100
Vial Holder for Mira M-1 Advanced PackageVial Holder for use with the Mira M-1 Advanced Package.
6.7503.100
MIRA Protective BootMIRA Protective Boot provides an extra layer of safety to MIRA devices. Made with a chemically resistant TPA material and specially designed to work with all SmartTip Attachments, the protective boot easily installs for a ruggedized feel and extra protection.
6.7503.110
PowerPack Protective BootPowerPack Protective Boot provides an extra layer of safety to PowerPack. Made with a chemically resistant TPA material and specially designed to work with Mira, the protective boot easily installs for a ruggedized feel and extra protection.
6.7503.120
Autofocus Standoff Grip KitAutofocus Standoff Grip Kit includes a picatinny rail, grip and mounting hardware for the AFSO.
6.7503.130
Autofocus Standoff Quick Release MountAutofocus Standoff Quick Release Mount is for standard picatinny rail mounting of the AFSO.
6.7520.000
Point-and-Shoot Adapter (SWD) for the Mira M-1 Advanced PackagePoint-and-Shoot Adapter (SWD) for the Mira M-1 Advanced Package with a focal length of 1.00 mm.
6.7520.010
Point-and-Shoot Adapter (LWD) for the Mira M-1 Advanced PackagePoint-and-Shoot Adapter (LWD) for the Mira M-1 Advanced Package with a focal length of 7.6 mm.
67530070
TacticID-1064 ST Wrist StrapWrist Strap for the Metrohm TacticID-1064 ST.
6.7550.000
ABS/TiO2 calibration standardABS/TiO2 standard for the calibration of the wavenumber scale of the Mira spectrometers.
6.7560.010
Protective Laser Glasses for MIRAProper laser safety precautions should be followed for the use of the MIRA products. Protection pursuant to EN 207 is offered with these protective glasses for the 785 nm laser excitation wavelength (also suitable for those who already wear eyeglasses). Work for long periods without difficulties, thanks to the lightweight construction and comfortable design of the protective laser glasses.
67560050
Laser Safety Goggles, 1064 nm WavelengthLaser Safety Goggles, 1064 nm Wavelength.
6.7560.200
MIRA PowerPack KitMIRA PowerPack Kit contains the MIRA PowerPack rechargeable external battery, a charger with USB-C socket, and a charger cable with USB-C plug. Designed for MIRA systems, the kit increases the period of usable charge to more than 8 hours.
6.7600.010
898 XYZ Sample Changer drip panDrip pan for 898 XYZ Sample Changer.
6.7600.020
898 XYZ Sample Changer rinsing station holderRinsing station holder for 898 XYZ Sample Changer.
6.7600.030
898 XYZ Sample Changer rinsing stationRinsing station for 898 XYZ Sample Changer.
6.7600.040
898 XYZ Sample Changer tubing guide898 XYZ Sample Changer tubing guide
6.7600.050
898 XYZ Sampler Changer titration head holder898 XYZ Sampler Changer titration head holder
6.7600.060
898 XYZ Sample Changer safety shield898 XYZ Sample Changer safety shield
6.7600.070
898 XYZ Sample Changer rinse and extraction kit898 XYZ Sample Changer rinse and extraction kit (FEP/TYGON).
6.7600.080
898 XYZ Sample Changer rinse reduction kit898 XYZ Sample Changer rinse reduction kit.
6.7600.090
898 XYZ Sample Changer 24 volt power supply unit898 XYZ Sample Changer 24 volt power supply unit.
6.9001.040
Paper for Custom DP40-S4N6.9001.050
Thermal paper for Custom Neos-N / Q3XThermal paper 60 mm / 25 m for Custom Neos-N / Q3X. New: 25-year legibility with correct storage.1 roll
6.9001.060
Paper roll for EPSON TM U220BPaper width: 76 mm, Paper length: 60 m
6.9001.070
Paper roll for TX-900MHPaper roll for TX-900MH impact printer
6.9001.080
Continuous adhesive labels for TX-900MHSelf-adhesive paper roll for TX-900MH impact printer
6.9002.050
Ink ribbon for Custom printerInk Ribbon
6.9002.060
Color ribbon for EPSON TM U220BNumber of characters: 3 million
6.9002.070
Color ribbon for TX-900MH impact printer6.9012.000
Dispersing aggregate for Polytron, 125 mmStandard dispersing aggregate for Polytron 1300 D
6.9012.010
Dispersing aggregate for Polytron, 157 mmSpecial dispersing aggregate (Metrohm version) with protruding knives
6.9013.000
Ionisation rod for ionizerThe ionisation rod is mounted with the holder (6.2057.160) to the 864 Robotic Balance Sample Processor.
6.9014.000
Debubbler for PILSTo remove the air bubbles prior to analysis.
6.9015.000
Evaporation chamber for KF Evaporator6.9015.010
Septum for KF-Evaporator 10x6.9015.020
Transfer tubing for KF Evaporator6.9914.137
Titration head for CSBTitration head for use in the CSB System (MATi 12). The titration head offers three retracted tubings with antidiffusion valve and one for aspiration of the titrated solution. The electrode can be fastened in place in an M10 screw connector. As before, three openings are provided for spray nozzles.
6.9914.139
Titration head with reinforced buret tipsTitration head with 3 reinforced buret tips, one M10 screw connection and one opening for an assembly (Polytron PT 1300 D).
6.9914.140
Robotic arm with holder for titration head and Polytron holder, right-swingingRobotic arm with holder for one titration head and one Polytron, for use with a 786 Swing Head.
6.9914.158
Dis-Cover titration headTitration head to 814 USB Sample Processor or for use in robotic arms with holder for titration head.
6.9915.078
Holder for transfer tubing, 25 mLThe 25 mL transfer tubing can be coiled up neatly and mounted on the guide chain of the Sample Processor with the help of the holder.
6.9915.079
Transfer tubing 25 mLThe 25 mL 2x M8 transfer tubing is mounted to the guide chain of the Sample Processor with the help of the 6.9915.078 holder
6.9920.141
Sample rack, 53 x 120 mL, (PP)Sample rack for 815 Robotic USB Sample Processor XL, 855 Robotic Titrosampler "Basic", suitable for 53 sample beakers. The following sample beakers can be used: 6.1459.300, 6.1459.307.Plastic: Polypropylene (PP)
6.9920.191
Sample rack, 35 x 60 mL and 3 x 250 mL (PVC)Sample rack for 858 Professional Sample Processor, 815 Robotic USB Sample Processor XL, suitable for 35 sample vessels and 3 rinsing bottles. The following sample vessels and rinsing bottles can be used: 6.1608.100, 60 mL and 250 mL Nalgene FEP vessels.Plastic: Polyvinyl chloride (PVC)
6.9920.231
Retaining plate for sample rack 159 x 2 mL + 3 x 300 mLPlate for deflecting the vessel cover on the Professional IC Sample Processor. For 2 mL sample vessels.
6.9920.252
Retaining plate for USB Sample Processor (2T), right6.9920.255
Sample rack 25 x 60 mL + 10 x 125 mLMulti-row sample rack for 25 samples in 60 mL Corning® cell culture flasks and 10 samples in 125 mL PE bottles (6.1627.000). Dedicated sample rack for trace analysis, e.g. in power plants.
6.9920.261
Holder for thermostatable titration vesselHolder for mounting a thermostatable titration vessel in the vicinity of the tower
6.9920.287
Sample rack, 109 x 11 mL and 12 x 125 mL (PVC)Sample rack for 858 Professional Sample Processor, 815 Robotic USB Sample Processor XL, suitable for 109 sample vessels and 12 standard bottles. The following sample vessels and standard bottles can be used: 6.2743.050, 6.1627.000, 6.2743.040.
6.9927.028
Safety shield for IC, right and leftSafety shield for 815 Robotic USB Sample Processor XL (2T/0P). Is utilized in IC when sample needles are used.
6.9927.031
Safety shield for USB Sample Processor (2T), for both towers6.9958.007
Overflow buret (100 mL) for Sample ProcessorOverflow buret for rapid and automatic measuring of 100 mL of sample and for sample transfer into an external titration vessel.
6.9958.125
34 mm titration head extension to Robotic Titrosampler "Light"Titration head extension to 855 Robotic Titrosampler "Light" for using the
6.9959.001
Injector with 1.0 µL internal loopFlat plate injector with 1.0 µL internal loop
A649281190
NIRS XDS Process Contact Lamp 50W, 12 Volt- White leadReplacement lamp with contact for NIRS Process instruments. 50W, 12 Volt- White lead.
A660044277
NIRS Analyzer PRO Lamp 12V/20WReplacement lamp for the NIRS Analyzer Pro (12V/20W)
ADC10M.S
Dual-channel ultra-fast sampling moduleThe ADC10M module is an ultra-fast sampling module that increases the sampling rate of the Autolab from 50 kSamples/s to 10 MSamples/s giving you the ability to acquire fast transients with intervals down to 100 ns.When combined with the SCAN250 module, you can perform ultra-fast cyclic voltammetry measurements with scan rates up to a practical limit of 250 kV/s, making it a powerful tool for studying fast kinetic processes.
ALL.CLIP.BLACK
Black Alligator ClampBlack alligator clamp for connections to electrodes in the electrochemical cell.
ALL.CLIP.RED
Red Alligator ClampRed alligator clamp for connections to electrodes in the electrochemical cell.
ALL.CLIP.SET
Set of crocodile clampsBlack or red crocodile clamps (sold individually) for connections to electrodes in the electrochemical cell.
AUT101.CASE
AUT101.CASEThe PGSTAT101 field case is designed to conveniently store or carry the Autolab PGSTAT101 and its components. The field case for PGSTAT101 provides room for the PGSTAT101, power cable, cell cable, monitor cable, NOVA Getting Started Manual and NOVA installation CD.
AUT204.CASE
Field case for PGSTAT204The PGSTAT204 field case is designed to conveniently store or carry the Autolab PGSTAT204 and its components. The field case for PGSTAT204 provides room for the PGSTAT204, power cable, dummy cell, cell cable, monitor cable, NOVA Getting Started Manual and NOVA installation CD.
AUT.COIN2.HLD.S
Autolab DuoCoin Cell HolderThe Autolab DuoCoin Cell Holder has 4-point Kelvin gold-plated contacts to assure the highest precision measurements for your battery research. A versatile accessory that can accommodate all standard cells sizes with capacity for smaller and larger non-standard cells and two cells can be processed at one time.Autolab DuoCoin Cell Holder gold plated contacts and gold plated PCB provide protection from corrosion and damage to the accessory in your busy laboratory.Experimental set up is simplified with the Autolab DuoCoin Cell Holder with visible electrode labels and cable connections that correspond to the Autolab potentionstat/galvanostat cable colors. Autolab’s attention to detail is reflected in the silicon surface grippers on the bottom of the Autolab DuoCoin Cell Holder to provide stability in a complex experiment set up.
AUT.DUMCELL.S
Autolab dummy cellDummy cell for instrument testing.
AUT.FIBER.200.UVIR
Autolab 200 μm optical fiber for UV/VIS/NIR applications.The Autolab spectrophotometer and light source are designed to connect to the electrochemical cell or cuvette holder using optical fibers. The standard dimensions of the optical fibers is 2 m in length and 200 μm in diameter. The fibers are fitted with SMA-905 connectors on both ends.
AUT.LED.BENCH.S
Autolab LED Driver optical benchOptical bench for measurements on photovoltaic devices. The allows for positioning of light source and detector.
AUT.LED.DRIVER.S
Autolab LED DriverSoftware controlled LED Driver for control of light source intensity. The LED Driver provides a maximum current of 700 mA and it can be used to power the LED lightsource provided with the Autolab LED Driver kit. The LED Driver can be programmed to provide a constant light output or a modulated light output.
AUT.LEDKIT.S
Autolab LED Driver KitThe Metrohm Autolab optical bench provides the means to study the electrochemical behavior of photovoltaic cells, like dye sensitized solar cells. The light source used in this setup is a highly focused LED. The bench includes a software programmable LED Driver which can be used to control the light source output.The light source itself is fitted with a quick release system, allowing a fast exchange of the light source and wavelength. It is supplied with a default 627 nm light source.
AUT.LED.LDC470.S
470 nm Blue LED CoverLED cover, with lens, fitted with a 470 nm LED (Blue) light source. Designed to fit the Autolab LED Driver kit. This cover allows electrochemical measurements under constant or modulated light.
AUT.LED.LDC505.S
505 nm Cyan LED CoverLED cover, with lens, fitted with a 505 nm LED (Cyan) light source. Designed to fit the Autolab LED Driver kit. This cover allows electrochemical measurements under constant or modulated light.
AUT.LED.LDC530.S
530 nm Green LED CoverLED cover, with lens, fitted with a 530 nm LED (Green) light source. Designed to fit the Autolab LED Driver kit. This cover allows electrochemical measurements under constant or modulated light.
AUT.LED.LDC590.S
590 nm Amber LED CoverLED cover, with lens, fitted with a 590 nm LED (Amber) light source. Designed to fit the Autolab LED Driver kit. This cover allows electrochemical measurements under constant or modulated light.
AUT.LED.LDC617.S
617 nm Red-Orange LED CoverLED cover, with lens, fitted with a 617 nm LED (Red-orange) light source. Designed to fit the Autolab LED Driver kit. This cover allows electrochemical measurements under constant or modulated light.
- 8.776.10128.776.1012Quick References 776 Dosimat, French
Andre sprog
- 8.776.10158.776.1015Quick References 776 Dosimat, Spanish
Andre sprog
- 8.776.10218.776.1021Instructions for Use 776 Dosimat, German
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- 8.776.10228.776.1022Instructions for Use 776 Dosimat, French
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- 8.776.10258.776.1025Instructions for use 776 Dosimat, Spanish
Andre sprog
- 8.776.30038.776.3003Declaration of conformity 776 Dosimat, English
English
- 8.778.30038.778.3003EU declaration of conformity 778 Sample Processor
English
- 8.780.30018.780.3001EU Declaration of conformity for 780 pH-meter
English
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- 8.781.30018.781.3001Declaration of conformity for 781 pH/ion meter
English
Andre sprog
- 8.781.30038.781.3003EU declaration of conformity 781 pH/Ion Meter
English
- 8.782.10018.782.1001Instructions for Use 782 IC Column Thermostat, german
Andre sprog
- 8.782.30038.782.3003Declaration of conformity 782 IC Column Thermostat, English
English
- 8.784.10018.784.1001Instructions for Use 784 KFP Titrino, german
Andre sprog
- 8.784.10028.784.1002Instructions for Use 784 KFP Titrino, french
Andre sprog
- 8.784.10058.784.1005Instructions for Use 784 KFP Titrino, spanish
Andre sprog
- 8.784.10118.784.1011Quick References 784 KFP Titrino, german
Andre sprog
- 8.784.10128.784.1012Quick References 784 KFP Titrino, french
Andre sprog
- 8.784.10158.784.1015Quick References 784 KFP Titrino, spanish
Andre sprog
- 8.784.10218.784.1021Short Instructions for Use 784 KFP Titrino, german
Andre sprog
- 8.784.10228.784.1022Short Instructions for Use 784 KFP Titrino, french
Andre sprog
- 8.784.10258.784.1025Short Instructions for Use 784 KFP Titrino, spanish
Andre sprog
- 8.784.30038.784.3003Declaration of conformity 784 KFP Titrino, english
English
- 8.785.10018.785.1001Instructions for Use 785 DMP Titrino, german
Andre sprog
- 8.785.10028.785.1002Instructions for Use 785 DMP Titrino, french
Andre sprog
- 8.785.10118.785.1011Quick References 785 DMP Titrino, german
Andre sprog
- 8.785.10218.785.1021Short Instructions for Use 785 DMP Titrino, german
Andre sprog
- 8.785.10238.785.1023Short Instructions for Use 785 DMP Titrino, english
English
- 8.785.30038.785.3003Declaration of conformity 785 DMP Titrino, english
English
- 8.786.17068.786.1706Leaflet "Dis-Cover Robotic arm" for 786 Swing head, German/French/English
English
Andre sprog
- 8.786.17168.786.1716Leaflet "KF Sample transfer set" for 786 Swing Head, German/French/English
English
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- 8.786.30038.786.3003EU declaration of conformity 786 Swing Head
English
Andre sprog
- 8.787.10018.787.1001Instructions for Use 787 KF Titrino, german
Andre sprog
- 8.787.10028.787.1002Instructions for Use 787 KF Titrino, french
Andre sprog
- 8.787.10058.787.1005Instructions for Use 787 KF Titrino, spanish
Andre sprog
- 8.787.10118.787.1011Quick References 787 KF Titrino, german
Andre sprog
- 8.787.10128.787.1012Quick References 787 KF Titrino, french
Andre sprog
- 8.787.10158.787.1015Quick References 787 KF Titrino, spanish
Andre sprog
- 8.787.30038.787.3003Declaration of conformity 787 KF Titrino, english
English
- 8.788.10018.788.1001Instructions for Use 788 IC Filtration Sample Processor, german
Andre sprog
- 8.788.10118.788.1011Quick Reference Guide 788 IC Filtration Sample Processor, german
Andre sprog
- 8.788.30038.788.3003Declaration of conformity 788 IC Filtration Sample Processor, english
English
- 8.789.10118.789.1011Quick References 778/789 (Robotic) Sample Processor, German
Andre sprog
- 8.789.10128.789.1012Quick References 778/789 (Robotic) Sample Processor, French
Andre sprog
- 8.789.10158.789.1015Quick References 778/789 (Robotic) Sample Processor, Spanish
Andre sprog
- 8.789.10218.789.1021Tutorial 778/789 (Robotic) Sample Processor, German
Andre sprog
- 8.789.10228.789.1022Tutorial 778/789 (Robotic) Sample Processor, French
Andre sprog
- 8.789.10238.789.1023Tutorial 778/789 (Robotic) Sample Processor, English
English
- 8.789.10258.789.1025Tutorial 778/789 (Robotic) Sample Processor, Spanish
Andre sprog
- 8.789.10618.789.1061Manual: 778/789 (Robotic) Sample Processor, German
Andre sprog
- 8.789.10628.789.1062Manual: 778/789 (Robotic) Sample Processor, French
Andre sprog
- 8.789.10658.789.1065Manual: 778/789 (Robotic) Sample Processor, Spanish
Andre sprog
- 8.789.30038.789.3003Declaration of conformity 789 Robotic Sampler Processor XL
English
- 8.790.10018.790.1001Instructions for Use 790 Personal IC, german
Andre sprog
- 8.790.10058.790.1005Instructions for Use 790 Personal IC, spanish
Andre sprog
- 8.790.10118.790.1011Supplement to Instructions for Use 790 Personal IC, german
Andre sprog
- 8.790.10128.790.1012Supplement to Instructions for Use 790 Personal IC, french
Andre sprog
- 8.790.10138.790.1013Supplement to Instructions for Use 790 Personal IC, english
English
- 8.790.10158.790.1015Supplement to Instructions for Use 790 Personal IC, spanish
Andre sprog
- 8.790.30038.790.3003Declaration of conformity 790 Personal IC, englisch
English
- 8.790.80178.790.8017Supplement to CD Metrodata 790 PC Software 1.0, german/english
English
Andre sprog
- 8.791.10118.791.1011Instructions for Use 791 VA Detector, german
Andre sprog
- 8.791.30038.791.3003Declaration of conformity 791 VA Detector, english
English
- 8.792.10028.792.1002Instructions for Use 792 Basic IC, french
Andre sprog
- 8.792.10118.792.1011Supplement to Instructions for Use 792 Basic IC, german
Andre sprog
- 8.792.10128.792.1012Supplement to Instructions for Use 792 Basic IC, french
Andre sprog
- 8.792.10138.792.1013Supplement to Instructions for Use 792 Basic IC, english
English
- 8.792.30038.792.3003Declaration of conformity 792 Basic IC, english
English
- 8.793.10018.793.1001Instructions for Use 793 IC Sample Preparation Module, german
Andre sprog
- 8.794.10018.794.1001Instructions for Use 794 Basic Titrino, german
Andre sprog
- 8.794.10028.794.1002Instructions for Use 794 Basic Titrino, french
Andre sprog
- 8.794.10058.794.1005Instructions for Use 794 Basic Titrino, spanish
Andre sprog
- 8.794.10118.794.1011Quick References 794 Basic Titrino, german
Andre sprog
- 8.794.10128.794.1012Quick References 794 Basic Titrino, french
Andre sprog
- 8.794.10158.794.1015Quick References 794 Basic Titrino, spanish
Andre sprog
- 8.794.30038.794.3003Declaration of conformity 794 Basic Titrino, english
English
- 8.795.10018.795.1001Instructions for Use 795 KFT Titrino, german
Andre sprog
- 8.795.10028.795.1002Instructions for Use 795 KFT Titrino, french
Andre sprog
- 8.795.10058.795.1005Instructions for Use 795 KFT Titrino, spanish
Andre sprog
- 8.795.10118.795.1011Quick References 795 KFT Titrino, german
Andre sprog
- 8.795.10128.795.1012Quick References 795 KFT Titrino, french
Andre sprog
- 8.795.10158.795.1015Quick References 795 KFT Titrino, spanish
Andre sprog
- 8.7951.0218.7951.021Short Instructions for Use 795 KFT Titrino, german
Andre sprog
- 8.795.10228.795.1022Short Instructions for Use 795 KFT Titrino, french
Andre sprog
- 8.795.10238.795.1023Short Instructions for Use 795 KFT Titrino, english
English
- 8.795.10258.795.1025Short Instructions for Use 795 KFT Titrino, spanish
English
- 8.795.30038.795.3003Declaration of conformity 795 KFT Titrino, english
English
- 8.796.10018.796.1001Instructions for Use 796 Titroprocessor, german
Andre sprog
- 8.796.10238.796.1023Tutorial 796 Titroprocessor, english
English
- 8.796.30038.796.3003Declaration of conformity 796 Titroprocessor, english
English
- 8.797.09038.797.0903EU declaration of conformity for 797 VA Computrace Software 1.0
English
- 8.797.09238.797.0923Declaration of conformity for 797 VA Computrace Software 1.2, English
English
- 8.797.09338.797.0933Declaration of conformity for 797 VA Computrace Software 1.3, English
English
- 8.797.30018.797.3001Declaration of conformity 797 VA Computrace
English
Andre sprog
- 8.798.10018.798.1001Instructions for Use 798 MPT Titrino, german
Andre sprog
- 8.798.10028.798.1002Instructions for Use 798 MPT Titrino, french
Andre sprog
- 8.798.10058.798.1005Instructions for Use 798 MPT Titrino, spanish
Andre sprog
- 8.798.10118.798.1011Quick References 798 MPT Titrino, german
Andre sprog
- 8.798.10128.798.1012Quick References 798 MPT Titrino, french
Andre sprog
- 8.798.10158.798.1015Quick References 798 MPT Titrino, spanish
Andre sprog
- 8.798.10218.798.1021Short Instructions for Use 798 MPT Titrino, german
Andre sprog
- 8.798.10228.798.1022Short Instructions for Use 798 MPT Titrino, french
Andre sprog
- 8.798.10238.798.1023Short Instructions for Use 798 MPT Titrino, english
English
- 8.798.10258.798.1025Short Instructions for Use 798 MPT Titrino, spanish
Andre sprog
- 8.798.30038.798.3003Declaration of conformity 798 MPT Titrino, english
English
- 8.799.10018.799.1001Instructions for Use 799 GPT Titrino, german
Andre sprog
- 8.799.10028.799.1002Instructions for Use 799 GPT Titrino, french
Andre sprog
- 8.799.10058.799.1005Instructions for Use 799 GPT Titrino, spanish
Andre sprog
- 8.799.10118.799.1011Quick References 799 GPT Titrino, german
Andre sprog
- 8.799.10128.799.1012Quick References 799 GPT Titrino, french
Andre sprog
- 8.799.10158.799.1015Quick References 799 GPT Titrino, spanish
Andre sprog
- 8.799.10218.799.1021Short Instructions for Use 799 GPT Titrino, german
Andre sprog
- 8.799.10228.799.1022Short Instructions for Use 799 GPT Titrino, french
Andre sprog
- 8.799.10238.799.1023Short Instructions for Use 799 GPT Titrino, english
English
- 8.799.10258.799.1025Short Instructions for Use 799 GPT Titrino, spanish
Andre sprog
- 8.799.30038.799.3003Declaration of conformity 799 GPT Titrino, english
English
- 8.800.30018.800.3001Declaration of conformity 800 Dosino
English
Andre sprog
- 8.801.30018.801.3001Declaration of Conformity for 801 Stirrer
English
Andre sprog
- 8.802.30018.802.3001Declaration of conformity 802 Stirrer
English
Andre sprog
- 8.803.30038.803.3003Declaration of conformity 803 Ti Stand
English
Andre sprog
- 8.804.30018.804.3001Declaration of Conformity for 804 Ti Stand
English
Andre sprog
- 8.805.30018.805.3001Declaration of conformity 805 Dosimat
English
Andre sprog
- 8.806.30018.806.3001EU declaration of Conformity for 806 Exchange Unit
English
Andre sprog
- 8.807.30018.807.3001EU declaration of Conformity for 807 Dosing Unit
English
Andre sprog
- 8.808.13018.808.1301Instructions for Use PC Control 1.0, german
Andre sprog
- 8.808.13028.808.1302Instructions for Use PC Control 1.0, french
Andre sprog
- 8.808.15018.808.1501Tutorial for PC Control 1.0, german
Andre sprog
- 8.808.15028.808.1502Tutorial for PC Control 1.0, french
Andre sprog
- 8.808.15038.808.1503Tutorial for PC Control 1.0, english
English
- 8.808.30338.808.3033Declaration of conformity 808 Titrando, english
English
- 8.809.30338.809.3033Declaration of conformity 809 Titrando, english
English
- 8.810.30018.810.3001Declaration of conformity 810 Sample Processor
English
Andre sprog
- 8.812.10018.812.1001Instructions for Use 812 Valve Unit, german
Andre sprog
- 8.813.10018.813.1001Instructions for Use 813 Compact Autosampler, German
Andre sprog
- 8.813.30038.813.3003Declaration of conformity 813 Compact Autosampler, English
English
- 8.814.30038.814.3003Declaration of conformity 814 USB Sample Processor
English
Andre sprog
- 8.815.17068.815.1706Leaflet "Ferrite cores" for 814/815 (Robotic) USB Sample Processor, German/French/English
English
Andre sprog
- 8.815.30038.815.3003Declaration of conformity 815 Robotic USB Sample Processor XL
English
Andre sprog
- 8.816.10018.816.1001Instructions for Use 816 IC Eluent Selector, german
Andre sprog
- 8.818.10218.818.1021Instructions for Use 818 IC Pump, german
Andre sprog
- 8.818.30038.818.3003Declaration of conformity 818 IC Pump, english
English
- 8.819.10118.819.1011Manual for 819 IC Detector/820 IC Separation Center, German
Andre sprog
- 8.819.30038.819.3003Declaration of conformity 819 IC Detector, english
English
- 8.820.30038.820.3003Declaration of conformity 820 IC Separation Center, english
English
- 8.822.10118.822.1011Instructions for Use 822 Titration Curve Simulator, german
Andre sprog
- 8.822.10128.822.1012Instructions for Use 822 Titration Curve Simulator, french
Andre sprog
- 8.822.10158.822.1015Instructions for Use 822 Titration Curve Simulator, spanish
Andre sprog
- 8.822.30018.822.3001EU declaration of Conformity for 822 Titration Curve Simulator
English
Andre sprog
- 8.823.30038.823.3003EU declaration of conformity 823 Membrane Pump Unit
English
Andre sprog
- 8.824.10018.824.1001Instructions for Use 824 Easy Sample Changer, German
Andre sprog
- 8.824.10028.824.1002Instructions for Use 824 Easy Sample Changer, French
Andre sprog
- 8.824.10058.824.1005Instructions for Use 824 Easy Sample Changer, Spanish
Andre sprog
- 8.824.11118.824.1111Quick References 824 Easy Sample Changer, German
Andre sprog
- 8.824.11128.824.1112Quick References 824 Easy Sample Changer, French
Andre sprog
- 8.824.11158.824.1115Quick References 824 Easy Sample Changer, Spanish
Andre sprog
- 8.824.30038.824.3003Declaration of conformity 824 Easy Sample Changer, English
English
- 8.825.09038.825.0903Declaration of conformity for 825 Lab Link + 825 Lab Link Server, english
English
- 8.825.10018.825.1001Instructions for Use 825 Lab Link, german
Andre sprog
- 8.826.30018.826.3001Declaration of conformity 826 pH mobile
English
- 8.827.12018.827.1201Quick reference guide for 826/827 pH meter, German
Andre sprog
- 8.827.12028.827.1202Quick reference guide for 826/827 pH meter, French
Andre sprog
- 8.827.12058.827.1205Quick reference guide for 826/827 pH meter, Spanish
Andre sprog
- 8.827.30018.827.3001Declaration of conformity 827 pH lab, english
English
Andre sprog
- 8.828.10018.828.1001Instructions for Use 828 IC Dual Suppressor, german
Andre sprog
- 8.828.10118.828.1011Supplement to Instructions for Use 828 IC Dual Suppressor, german
Andre sprog
- 8.828.10138.828.1013Supplement to Instructions for Use 828 ID Dual Suppressor, english
English
- 8.828.30038.828.3003Declaration of conformity 828 IC Dual Suppressor, english
English
- 8.830.10018.830.1001Instructions for Use 830 IC Interface, german
Andre sprog
- 8.830.30038.830.3003Declaration of conformity 830 IC Interface, english
English
- 8.831.10018.831.1001Instructions for Use 756/831 KF Coulometer, german
Andre sprog
- 8.831.10028.831.1002Instructions for Use 756/831 KF Coulometer, french
Andre sprog
- 8.831.10058.831.1005Instructions for Use 756/831 KF Coulometer, spanish
Andre sprog
- 8.831.10118.831.1011Quick References 756/831 KF Coulometer, german
Andre sprog
- 8.831.10128.831.1012Quick References 756/831 KF Coulometer, french
Andre sprog
- 8.831.10158.831.1015Quick References 756/831 KF Coulometer, Spanish
Andre sprog
- 8.831.30038.831.3003EU declaration of conformity 831 KF Coulometer
English
Andre sprog
- 8.832.10118.832.1011Short introduction 832 KF Thermoprep, german
Andre sprog
- 8.832.10128.832.1012Short introduction 832 KF Thermoprep, french
Andre sprog
- 8.832.10158.832.1015Short introduction 832 KF Thermoprep, spanish
Andre sprog
- 8.832.10218.832.1021Instrctions for Use 832 KF Thermoprep, german
Andre sprog
- 8.832.10228.832.1022Instructions for use 832 KF Thermoprep, french
Andre sprog
- 8.832.10258.832.1025Instructions for Use 832 KF Thermoprep, spanish
Andre sprog
- 8.832.30038.832.3003Declaration of conformity 832 KF Thermoprep, english
English
- 8.833.10018.833.1001Instructions for Use 833 IC Liquid Handling Unit, german
Andre sprog
- 8.833.30038.833.3003Declaration of conformity 833 IC Liquid Handling Unit, english
English
- 8.835.30238.835.3023Declaration of conformity 835 Titrando, english
English
- 8.836.30238.836.3023Declaration of conformity 836 Titrando, english
English
- 8.837.10018.837.1001Instructions for Use 837 IC Degasser, german
Andre sprog
- 8.837.30018.837.3001Declaration of conformity 837 IC Degasser
English
- 8.838.10118.838.1011Manual for 838 Advanced Sample Processor, German
Andre sprog
- 8.838.10128.838.1012Instructions for Use 838 Advanced Sample Processor, French
Andre sprog
- 8.838.13118.838.1311Installation Instruction 838 Advanced Sample Processor, German
Andre sprog
- 8.838.13278.838.1327Leaflet for installation 838 Advanced Sample Processor, German/English
English
Andre sprog
- 8.838.30038.838.3003EU declaration of conformity 838 Advanced Sample Processor
English
Andre sprog
- 8.838.60118.838.6011Brochure: 838 Advanced VA Sample Processor
The 838 Advanced VA Sample Processor allows the fully automatic and extremely flexible processing of large sample series in the routine monitoring of electroplating baths.
Andre sprog
- 8.840.09038.840.0903Declaration of conformity PC Control 4.0, english
English
- 8.840.09238.840.0923Declaration of conformity PC Control 4.1, english
English
- 8.840.09338.840.0933Declaration of conformity Touch Control Software, english; program versions 5.808.0141 / 5.809.0141 / 5.840.0131
English
- 8.840.11318.840.1131Installation Instructions for Titrando, german
Andre sprog
- 8.840.11328.840.1132Installation Instructions for Titrando, french
Andre sprog
- 8.840.11358.840.1135Installation Instructions for Titrando, spanish
Andre sprog