The determination of PBBE (tetrabromobisphenol A - TBBPA, octabromodiphenyl ether - OCTA and decabromodiphenyl ether - DECA) in a polymer sample was carried out with the Nucleosil EC - 250 mm column; for this purpose a methanol and phosphate buffer was used as an eluent and subjected to UV detection in accordance with the IEC 62321 method for RoHS testing.