Automated volumetric KF titration including sample preparation

Automated volumetric KF titration including sample preparation
Part Number: MATi 11

Fully automated system for volumetric Karl Fischer water content determination in up to 53 samples. This system is controlled with tiamo™ and consists of an 815 Robotic USB Sample Processor XL, a 901 Titrando, a Polytron PT 1300 D and extensive accessories.

The samples are weighed out into beakers, sealed to protect against humidity and placed on the rack. Before the actual titration, a defined volume of KF reagent is added and the sample is pulverized with the help of a Polytron. The water that is released is titrated afterwards. Even samples of poor solubility, e.g., tablets, can be analyzed without difficulty with this method. The use of solubility promoters can be avoided in this way.

  • Documentos
  • Peças
  • Water determination according to Karl Fischer with MATi 11 – Complete system for fully automated, volumetric Karl Fischer titration, including sample preparation (english)
    • Wassergehaltsbestimmung nach Karl Fischer mit MATi 11 – Vollautomatisches Komplettsystems für die volumetrische Karl-Fischer-Titration einschliesslich Probenvorbereitung (deutsch)

Faça o download do escopo completo de entrega e acessórios opcionais

  • Polytron PT 1300 D
    2.136.0100
    Polytron PT 1300 D

    Polytron PT 1300 D - Metrohm version

    Homogenizer that can be controlled directly by tiamo™ or Touch Control.

    The Polytron PT 1300 D is comprised of a monitoring instrument and a drive. The coupling system on the drive permits the simple and rapid replacement of the aggregates without additional tools.
    Solid samples can be pulverized without difficulty. The instrument is however outstandingly suitable for ensuring thorough mixing in viscous samples.

    1 piece(s)

  • 
    772 Pump Unit – aspirate
    2.772.0120
    772 Pump Unit – aspirate

    Peristaltic pump for direct connection to Sample Processors. The "Aspiration" version contains extensive accessories for the aspiration of titered-out solutions.


    1 piece(s)

  • 786 Swing Head
    2.786.0040
    786 Swing Head
    Additional equipment for Robotic Sample Processors XL without titration or transfer heads.

    2 piece(s)

  • 800 Dosino
    2.800.0010
    800 Dosino

    Drive with write/read hardware for intelligent Dosing Units. With fixed cable (length 150 cm).

    2 piece(s)

  • 815 Robotic USB Sample Processor XL (2T/0P)
    2.815.0130
    815 Robotic USB Sample Processor XL (2T/0P)

    Robotic USB Sample Processor XL for the automatic processing of routine samples in series with large quantities and for complex sample preparation or parallel runs. Up to four pumps (membrane or peristaltic) and three dosing devices for Liquid Handling tasks can be connected.

    Because of the multitude of application variants, rack, stirrer, titration head, robotic arm, Swing Head and sample vessels must be tailored to the application and ordered separately.
     

     

    1 piece(s)

  • 901 Titrando
    2.901.0010
    901 Titrando

    The Karl Fischer Titrando for the modern titration laboratory

    In addition to the Karl Fischer mode (KFT), the high-end titrator is also equipped with the SET mode and can thus perform titrations to a predefined endpoint.

    "iTrode ready": As a result of the high-resolution, galvanic measuring interface – now also for the first time with additional digital measuring input for the intelligent "iTrodes" electrodes – it is additionally possible to perform pH measurements with a maximum of precision.

    Thanks to the four MSB connectors, up to four Dosinos can be connected to the 901 Titrando. These can be used not only for titration, but also for the automated addition of sample, standard and auxiliary solutions such as solubility promoters. Furthermore, you have all of the Liquid Handling commands at your disposal, which means that the aspiration of exhausted reagent and the addition of fresh solvent can also be automated.

    1 piece(s)

  • Sample beakers, plastic (PP), 120 mL / 250 pieces 
    6.1459.300
    Sample beakers, plastic (PP), 120 mL / 250 pieces 

    Sample beakers, plastic (polypropylene, PP), 120 mL, suitable for sample racks 6.2041.470, 6.2041.840, 6.2041.850, 6.2068.010, 6.2068.020, 6.2068.030 and 6.9920.141, 250 pieces
     

    1 piece(s)

  • Robotic arm with transfer head for 786 Swing Head, left swinging
    6.1462.030
    Robotic arm with transfer head for 786 Swing Head, left swinging
    Transfer robotic arm for liquid handling purposes

    1 piece(s)

  • FEP tubing / M6 / 100 cm
    6.1805.120
    FEP tubing / M6 / 100 cm
    With light and kink protection

    2 piece(s)

  • Adapter M6 / M8 inner
    6.1808.230
    Adapter M6 / M8 inner
    Adapter with M6 and M8 inner threads

    1 piece(s)

  • Aspiration tube
    6.1821.000
    Aspiration tube
    For KF Sampler

    1 piece(s)

  • Foil holder
    6.2037.080
    Foil holder
    Foil holder for 120 mL PP beaker (6.1459.300)

    53 piece(s)

  • Cable RS-232 DB9 socket f – DB9 plug
    6.2134.110
    Cable RS-232 DB9 socket f – DB9 plug
    Connecting Metrohm RS-232 interface (DB9) to a Custom DP40 printer. For Titrinos or 756/831 KF Coulometer. RS-232 extension cable (1:1)

    1 piece(s)

  • Cable USB A – mini-DIN 8-pin
    6.2151.000
    Cable USB A – mini-DIN 8-pin
    Controller cable

    1 piece(s)

  • Drip pan for 789/815/855
    6.2711.070
    Drip pan for 789/815/855
    Drip pan for 789, 815, 855 Robotic Sample Processors XL

    1 piece(s)

  • Al foil
    6.2820.000
    Al foil
    1000 circular sheets of 80 mm diameter. Thickness: 0.010 mm. Used together with 6.2037.030 Foil holder for 6.1432.210 Sample beaker. For 674 KF Sample Changer

    1 piece(s)

  • Dosing Unit 10 mL
    6.3032.210
    Dosing Unit 10 mL
    Dosing unit with integrated data chip with 10 mL glass cylinder and light protection, mountable on reagent bottle with ISO/DIN GL45 thread. FEP tubing connection, anti-diffusion buret tip.

    1 piece(s)

  • Dosing Unit 50 mL
    6.3032.250
    Dosing Unit 50 mL
    Dosing unit with integrated data chip with 50 mL glass cylinder and light protection, mountable on reagent bottle with ISO/DIN GL45 thread. FEP tubing connection, anti-diffusion buret tip.

    1 piece(s)

  • Tiamo 2.5 Full CD: 1 license
    6.6056.252
    Tiamo 2.5 Full CD: 1 license

    Computer program for controlling complex titration systems.

    • Graphical method editor with numerous templates
    • Layout manager for individual monitor interface
    • Professional database with reevaluation
    • Export to LIMS, NuGenesis, Cyberlab, etc.
    • High-performance report generator
    • In compliance with the directives according to FDA 21 CFR Part 11
    • Parallel titration
    • Dialog languages: German, English, French, Italian, Spanish, Portuguese, Polish, Russian, Slovakian, Czech, Japanese, Chinese and Traditional Chinese

     

    1 piece(s)

  • Dispersing aggregate for Polytron, 157 mm
    6.9012.010
    Dispersing aggregate for Polytron, 157 mm
    Special dispersing aggregate (Metrohm version) with protruding knives

    1 piece(s)

  • KF indicator electrode for automation
    6.9903.048
    KF indicator electrode for automation

    Double platinum wire electrode for automation with fixed cable, plug F

    1 piece(s)

  • Titration head with reinforced buret tips
    6.9914.139
    Titration head with reinforced buret tips

    Titration head with 3 reinforced buret tips, one M10 screw connection and one opening for an assembly (Polytron PT 1300 D).

    1 piece(s)

  • Robotic arm with holder for titration head and Polytron holder, right-swinging
    6.9914.140
    Robotic arm with holder for titration head and Polytron holder, right-swinging

    Robotic arm with holder for one titration head and one Polytron, for use with a 786 Swing Head.

    1 piece(s)

  • Sample rack 53 x 120 mL, PP
    6.9920.141
    Sample rack 53 x 120 mL, PP

    Sample rack for 53 x 120 mL sample vessels (6.1459.300) with foil holder (6.2037.080), multi-row

    1 piece(s)